Experiment 1: Spatulation Rx Camphor 0.06 g Salol 0.20 g Adsorbents 0.20 g Light Magnesium Oxide Magnesium Carbonate Cornstarch Kaolin * The prescription is to be prepared in two methods: Method A: 1. Weigh the reagent individually and label. 2. Triturate camphor with half of the amount of the adsorbents. 3. Separately triturate salol with the other half of the adsorbents. 4. Mix the two resulting powders together with light trituration. 5. Note the consistency of the mixture right after step 4. 6. Enclose half of the mixture in a wax paper and the other half in plastic cellophane, then store for a week. 7. Note the consistency of the mixtures in both packaging. 8. Fill in the data in the table of results then conclude. Method B: 1. Weigh the reagent individually and label. 2. Triturate the salol and camphor together to form a pasty mass. 3. Add the adsorbents, then triturate the mixture lightly. 4. Note the consistency of the mixture right after step 4. 5. Enclose half of the mixture in a wax paper and the other half in plastic cellophane, then store for a week. 6. Note the consistency of the mixtures in both packaging. 7. Fill in the data in the table of results then conclude. Procedures Observations After mixing After one week of storage Wax paper Plastic cellophane Method A Damp powder Dry powder Cement-like mass Method B Soft mass or liquid- like Soft mass or liquid-like Slightly damp powder Question 1: What is the weight of each adsorbent used in each method? Show your complete handwritten solution (please insert a clear and well-lit image on the space provided; no reference required) to justify your answer.

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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Experiment 1: Spatulation

Rx Camphor 0.06 g
Salol 0.20 g
Adsorbents 0.20 g
Light Magnesium Oxide
Magnesium Carbonate
Cornstarch
Kaolin

* The prescription is to be prepared in two methods:
Method A:
1. Weigh the reagent individually and label.
2. Triturate camphor with half of the amount of the adsorbents.
3. Separately triturate salol with the other half of the adsorbents.
4. Mix the two resulting powders together with light trituration.
5. Note the consistency of the mixture right after step 4.
6. Enclose half of the mixture in a wax paper and the other half in plastic cellophane, then store for a week.
7. Note the consistency of the mixtures in both packaging.
8. Fill in the data in the table of results then conclude.

Method B:
1. Weigh the reagent individually and label.
2. Triturate the salol and camphor together to form a pasty mass.
3. Add the adsorbents, then triturate the mixture lightly.
4. Note the consistency of the mixture right after step 4.
5. Enclose half of the mixture in a wax paper and the other half in plastic cellophane, then store for a week.
6. Note the consistency of the mixtures in both packaging.
7. Fill in the data in the table of results then conclude.
Procedures

Observations

After mixing After one week of storage
Wax paper Plastic cellophane
Method A Damp powder Dry powder Cement-like mass
Method B Soft mass or liquid-

like Soft mass or liquid-like Slightly damp powder

Question 1: What is the weight of each adsorbent used in each method? Show your complete handwritten solution (please insert a clear and well-lit image on the space
provided; no reference required) to justify your answer.

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