Elucidate the structure for compound B using spectroscopic data provided. B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D₂O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (i) Identify the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance? MS: m/z: 86 (10%): 87 (0.5); 68.07 ( 100.0%), 69.08 (5.4%) 1H NMR (d): 5.67 (1H, doublet, J= 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet). 1.63 (3H, doublet), 1.07 (3H, doublet). IR (see below) 100 VULZONBALVONAL 4000 3000 2000 RAVENUISERI 1500 1000 500

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Elucidate the structure for compound B using spectroscopic data provided.
B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D₂O shake). i) Provide the Molecular
formula, (ii) Identify the correct structure (i) Identify the most important (diagnostic) IR signal(s) and match each proton NMR
absorption with the proton that is causing that absorbance?
MS: m/z: 86 (10%): 87 (0.5); 68.07 ( 100.0%), 69.08 (5.4%)
1H NMR (d): 5.67 (1H, doublet, J= 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet). 1.63 (3H, doublet), 1.07 (3H, doublet).
IR (see below)
100
TRANSALANCER
4000
3000
2000
RAVENUISERI
1500
1000
500
Transcribed Image Text:Elucidate the structure for compound B using spectroscopic data provided. B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D₂O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (i) Identify the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance? MS: m/z: 86 (10%): 87 (0.5); 68.07 ( 100.0%), 69.08 (5.4%) 1H NMR (d): 5.67 (1H, doublet, J= 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet). 1.63 (3H, doublet), 1.07 (3H, doublet). IR (see below) 100 TRANSALANCER 4000 3000 2000 RAVENUISERI 1500 1000 500
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