efer attachment) (a) Sketch a process flow diagram (PFD) of the process described above.

Introduction to Chemical Engineering Thermodynamics
8th Edition
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Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
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Chapter1: Introduction
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A small plant is designed for conversion of component A to a target product of component B. Component A is fed from a holding tank where it is mixed with recycled component A. The Component A is pumped and heated to reaction temperature before entering the reactor. The reaction of component A does not require a catalyst, since it is initiated at high temperatures. The reactor is simply a vessel with inert packing to promote radial mixing. The reaction is quenched and main products formed consist of component B and C while side reaction of some component B has produced component D. There is one holding vessels is used to hold reaction products and remove component D. This allows a continuous flow of other components into distillation column (column 1) where the component A is separated (as bottom product) and recycled, and another distillation column (column 2) was used to purify component B (less volatile) from the component C. The recycle component A will be cooled and drive to the holding tank as mention earlier. The important conditions for equipment described above are summarized in Table 1 below.

(Refer attachment)

(a) Sketch a process flow diagram (PFD) of the process described above.
(b) Then, construct process conditions matrix (PCM) for the process and determine all conditions of special concern. For each condition of special concern identified, suggest at least one reason why such a condition was used and process alternative to eliminate the condition.

 

Equipment
Holding tank (Fed component A)
Table 1: Inlet and outlet condition of the major equipment
Holding vessel (product mixture)
Heater
Reactor
aCooler (reactor effluent)
*Cooler (recycle stream)
Distillation column 1
Distillation column 2
Inlet
25 °C (fresh fed)
170 °C (recycle fed)
110 kPa
175 °C
148 kPa
150 °C
230 kPa
380 °C
196 kPa
342.8 °C
183 kPa
345 °C
90 kPa
175 °C
136 kPa
108 °C
125 kPa
Outlet
150 °C
105 kPa
175 °C
136 kPa
380 °C
196 kPa
343 °C
183 kPa
175 °C
148 kPa
170 °C
65 kPa
Top: 108 °C
125 kPa
Bottom: 345 °C
90 kPa
Top: 119 °C
105 kPa
Bottom: 253 °C
125 kPa
a Bfw (115 °C) is used to cool the stream and leave as Ips (160 °C) for both heat exchanger
Transcribed Image Text:Equipment Holding tank (Fed component A) Table 1: Inlet and outlet condition of the major equipment Holding vessel (product mixture) Heater Reactor aCooler (reactor effluent) *Cooler (recycle stream) Distillation column 1 Distillation column 2 Inlet 25 °C (fresh fed) 170 °C (recycle fed) 110 kPa 175 °C 148 kPa 150 °C 230 kPa 380 °C 196 kPa 342.8 °C 183 kPa 345 °C 90 kPa 175 °C 136 kPa 108 °C 125 kPa Outlet 150 °C 105 kPa 175 °C 136 kPa 380 °C 196 kPa 343 °C 183 kPa 175 °C 148 kPa 170 °C 65 kPa Top: 108 °C 125 kPa Bottom: 345 °C 90 kPa Top: 119 °C 105 kPa Bottom: 253 °C 125 kPa a Bfw (115 °C) is used to cool the stream and leave as Ips (160 °C) for both heat exchanger
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