Discuss the relationship between boiling point of 1,1-dichlorobutane; 1,2-dichlorobutane; 1,3-dichlorobutane; 1,4-dichlorobutane and their retention time in gas chromatography. Injection Date: 1/26/2023 5:23:33 PMMethodLast changedPA80000070000060000050000089400000300000200000123456710000001111Totals :||:: 1/25/2023 5:40:34 PM by SYSTEMFID1 A, Front Signal (no Sample Name (front) (1) 2023-01-26 17-23-33.D)||111111111111111111||11||Inj Volume: ManuallyC:\USERS\PUBLIC\DOCUMENTS\CHEMSTATION\1\METHODS\Dichlorobutanes.M11||11||||||||111111110.511:||-0.680Signal 1: FID1 A, Front SignalPeak RetTime Type Width#[min][min]----|-------|----|-----0.700-1>0.8180.8850.963Signal1.00001.00000.917Area[pA*s]Area Percent Report0.680 BV S 0.0124 9.54562e40.700 VB S0.818 VV T0.885 VV T0.917 VV T0.963 VV T0.995 VV T1.326 VV T2.060 VB0.995111||111111Sorted ByMultiplierDilution:Do not use Multiplier & Dilution Factor with ISTDSHeight[PA]11111.24677e6 1.08641e6111111111.326||11||||111111Area81.511111.28873e57.656290.0224 9.40780e5 7,00365e5 75.457380.0114 9929.71875 1.41214e40.796440.0172 2888.63208 2726.904790.231690.0119 4.17981e4 5.59483e43.352510.468460.0178 5840.57568 5254.354491.22904 e50.0125 9.75613e47.825130.0149 5.09791e4 5.46976e44.088900.0158 1536.15088 1519.26013 0.1232111||||1111||111111||111122.0602.5 min

Ans. The boiling of given compound are given in table below Compound Boiling point…

Answered: Discuss the relationship between…

Discuss the relationship between boiling point of 1,1-dichlorobutane; 1,2-dichlorobutane; 1,3-dichlorobutane; 1,4-dichlorobutane and their retention time in gas chromatography.

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter8: Sampling, Standardization, And Calibration

Section: Chapter Questions

Problem 8.12QAP

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Question

100%

Discuss the relationship between boiling point of 1,1-dichlorobutane; 1,2-dichlorobutane; 1,3-dichlorobutane; 1,4-dichlorobutane and their retention time in gas chromatography.

Injection Date: 1/26/2023 5:23:33 PM
Method
Last changed
PA
800000
700000
600000
500000
8
9
400000
300000
200000
1
2
3
4
5
6
7
100000
0
11
11
Totals :
||
:
: 1/25/2023 5:40:34 PM by SYSTEM
FID1 A, Front Signal (no Sample Name (front) (1) 2023-01-26 17-23-33.D)
||
11
11
11
11
11
11
11
11
11
||
11
||
Inj Volume: Manually
C:\USERS\PUBLIC\DOCUMENTS\CHEMSTATION\1\METHODS\Dichlorobutanes.M
11
||
11
||
||
||
||
11
11
11
11
0.5
11
:
||
-0.680
Signal 1: FID1 A, Front Signal
Peak RetTime Type Width
#
[min]
[min]
----|-------|----|-----
0.700
-1
>0.818
0.885
0.963
Signal
1.0000
1.0000
0.917
Area
[pA*s]
Area Percent Report
0.680 BV S 0.0124 9.54562e4
0.700 VB S
0.818 VV T
0.885 VV T
0.917 VV T
0.963 VV T
0.995 VV T
1.326 VV T
2.060 VB
0.995
1
11
||
11
11
11
Sorted By
Multiplier
Dilution
:
Do not use Multiplier & Dilution Factor with ISTDS
Height
[PA]
11
11
1.24677e6 1.08641e6
11
11
11
11
1.326
||
11
||
||
11
11
11
Area
8
1.5
11
11
1.28873e5
7.65629
0.0224 9.40780e5 7,00365e5 75.45738
0.0114 9929.71875 1.41214e4
0.79644
0.0172 2888.63208 2726.90479
0.23169
0.0119 4.17981e4 5.59483e4
3.35251
0.46846
0.0178 5840.57568 5254.35449
1.22904 e5
0.0125 9.75613e4
7.82513
0.0149 5.09791e4 5.46976e4
4.08890
0.0158 1536.15088 1519.26013 0.12321
11
||
||
11
11
||
11
11
11
||
11
11
2
2.060
2.5 min

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