Design experimental set-ups that will maximize the yield and purity of the Butyl Acetate. Included the discussion of the Chemistry behind the synthesis as well as safe laboratory techniques and practices to synthetic design

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Design experimental set-ups that will maximize the yield and purity of the Butyl Acetate. Included the discussion of the Chemistry behind the synthesis as well as safe laboratory techniques and practices to synthetic design.

 

I.
MATERIALS
CAS # or Catalogue # from a supplier
(Example: Sigma Aldrich)
Chemicals / Reagents
Apparatus / Equipment (Indicate below)
I.
EXPERIMENTAL PROCEDURE
II.
DISCUSSION
(Explain the Chemistry behind the synthesis process.)
IV.
CHEMICAL SAFETY AND WASTE DISPOSAL
Hazard Classification and
Handling Safety Precautions
Disposal Procedure
(Describe briefly.)
Chemicals /
Reagents
Transcribed Image Text:I. MATERIALS CAS # or Catalogue # from a supplier (Example: Sigma Aldrich) Chemicals / Reagents Apparatus / Equipment (Indicate below) I. EXPERIMENTAL PROCEDURE II. DISCUSSION (Explain the Chemistry behind the synthesis process.) IV. CHEMICAL SAFETY AND WASTE DISPOSAL Hazard Classification and Handling Safety Precautions Disposal Procedure (Describe briefly.) Chemicals / Reagents
STEP 1
heat
H2C=C=O
CH3-
acetic anhydride
ethenone
acetic acid
OH
H3C
CH3
STEP 2
cat.
ethyl acetate
OH
H3C
CH3
H3C
CH3
ethanol
acetic anhydride
STEP 3
OH
butanol
CH3:
butyl acetate
cat.
H3C
`CH3
acetic acid
OH
H3C°
CH3
ethyl acetate
Transcribed Image Text:STEP 1 heat H2C=C=O CH3- acetic anhydride ethenone acetic acid OH H3C CH3 STEP 2 cat. ethyl acetate OH H3C CH3 H3C CH3 ethanol acetic anhydride STEP 3 OH butanol CH3: butyl acetate cat. H3C `CH3 acetic acid OH H3C° CH3 ethyl acetate
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