d) The ¹HNMR spectrum OF 4-hydroxybenzaldehyde is shown below, with the spectroscopic details summarized in the table that follows. Use this data to answer questions i) to iii). Chemical Shift (ppm) 10 9.92 9.71 7.79 6.89 8 Splitting/Multiplicity singlet singlet (broad) doublet doublet PPM i) The signal at 9.71 ppm is produced by the proton(s) at location Blank 1 ii) The signal at 7.79ppm is produced by the proton(s) at location Blank 2 iii) The signal at 6.89ppm is produced by the proton(s) at location Blank 3 HO B Integration B 2 1H 1H 2H 2H O O H₂ ⠀

Organic Chemistry: A Guided Inquiry
2nd Edition
ISBN:9780618974122
Author:Andrei Straumanis
Publisher:Andrei Straumanis
ChapterL4: Proton (1h) Nmr Spectroscopy
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d) The ¹HNMR spectrum OF 4-hydroxybenzaldehyde is shown below, with the spectroscopic details summarized in the table that
follows. Use this data to answer questions i) to iii).
Chemical Shift (ppm)
10
9.92
9.71
7.79
6.89
8
Splitting/Multiplicity
singlet
singlet (broad)
doublet
doublet
PPM
i) The signal at 9.71 ppm is produced by the proton(s) at location Blank 1
ii) The signal at 7.79ppm is produced by the proton(s) at location Blank 2
iii) The signal at 6.89ppm is produced by the proton(s) at location Blank 3
OH
Integration
B
2
1H
1H
2H
2H
O
⠀
HD
Transcribed Image Text:d) The ¹HNMR spectrum OF 4-hydroxybenzaldehyde is shown below, with the spectroscopic details summarized in the table that follows. Use this data to answer questions i) to iii). Chemical Shift (ppm) 10 9.92 9.71 7.79 6.89 8 Splitting/Multiplicity singlet singlet (broad) doublet doublet PPM i) The signal at 9.71 ppm is produced by the proton(s) at location Blank 1 ii) The signal at 7.79ppm is produced by the proton(s) at location Blank 2 iii) The signal at 6.89ppm is produced by the proton(s) at location Blank 3 OH Integration B 2 1H 1H 2H 2H O ⠀ HD
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