C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen 2.dx Normal 13C spectrum Assign all signals individually. You will need the HSQC to do this. C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen 3.dx DEPT135 spectrum - CH,CH3 are opposite phase to CH2 Quaterary carbons do not appear. C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen_4.dx DEPT 90 Spectrum. Only CH appear 6 7 9 10 8 5 11 LOH 3 4 1 2 210 200 190 180 170 160 150 140 130 120 110 100 90 f1 (ppm) 8- 80 -8 70 -60 60 - 50 40 -3 -2 ignore small peaks 30 -30 -20 10 0 -10 -1
C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen 2.dx Normal 13C spectrum Assign all signals individually. You will need the HSQC to do this. C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen 3.dx DEPT135 spectrum - CH,CH3 are opposite phase to CH2 Quaterary carbons do not appear. C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen_4.dx DEPT 90 Spectrum. Only CH appear 6 7 9 10 8 5 11 LOH 3 4 1 2 210 200 190 180 170 160 150 140 130 120 110 100 90 f1 (ppm) 8- 80 -8 70 -60 60 - 50 40 -3 -2 ignore small peaks 30 -30 -20 10 0 -10 -1
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
Assign all the signals individually (please assign the red, green and blue)

Transcribed Image Text:C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen 2.dx
Normal 13C spectrum Assign all signals individually.
You will need the HSQC to do this.
C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen 3.dx
DEPT135 spectrum - CH,CH3 are opposite phase to CH2
Quaterary carbons do not appear.
C:/Users/rvanhoveln/Documents/CHEM 352L/2019/Ibuprofen part 2/RVH Ibuprofen_4.dx
DEPT 90 Spectrum. Only CH appear
6
7
9
10
8
5
11
LOH
3
4
1
2
210 200 190 180 170 160
150
140 130 120
110
100 90
f1 (ppm)
8-
80
-8
70
-60
60
-
50 40
-3
-2
ignore small peaks
30
-30
-20
10
0
-10
-1
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