compare all the trials, which solvent provided the best separation of these color components? which solvent is the worst in separation? explain the difference in terms of intermolecular forces to the best of your knowledge

Appl Of Ms Excel In Analytical Chemistry
2nd Edition
ISBN:9781285686691
Author:Crouch
Publisher:Crouch
Chapter14: Chromatography
Section: Chapter Questions
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compare all the trials, which solvent provided the best separation of these color components? which solvent is the worst in separation? explain the difference in terms of intermolecular forces to the best of your knowledge

MATERIALS
Safety goggles
pencil, ruler and scissors
methanol
chromatography paper
plastic wash bottle
ethanol
4 50ml graduated cylinder
food coloring mixture
2-propanol
4 cork stoppers
distilled water
acetic acid
4 wire paper clips
ethyl acetate
1 capillary tube
cyclohexane
PROCEDURE
1.
Using a ruler; draw a straight pencil line across the chromatography paper, about 1.5cm from the bottom.
2.
Use the capillary tube to put one small drop of dye on the pencil line. Let it dry. Repeat step 1-2 for other 3
trials with different developing solvents.
3.
Fill each of four 50ml graduated cylinders with four different solvents you choose to about 5 ml. Use a cork
stopper to suspend each filter paper strip in a graduated cylinder, as shown in Figure 4.1. The end of the filter
paper should be below the solvent level; the dye spot should be above the solvent level.
Permit the solvent in each graduated cylinder to rise up the filter paper until it is about 2cm from the top of
4.
partices, (atoms or Tonst
Remove the strips from the graduated cylinders. Using a pencil, mark on each strip the distance the solvent
uncan u
the paper.
5.
has traveled from the point of origin. Record these distances as D; in a data table.
6.
Measure on each paper strip the distance each dye spot has traveled. Record these distances as Dş. If the
original dye spot has separated into several spots, measure and record the D, for each spot. Calculate the Rf
value for each components in the dye for all trails.
7.
Dispose and recycle materials according to teacher's instruction.
Paper
chp
hooh
Solvent
front
Figure 4.1 the apparatus
with distill H2Q H-bonds
With ethyl acetate: DDF & H-bm
WEth Cyclohexane: LDF
gwith 2-propanut: H-bonding.
Solvent
Allura Red YSI
Brilliant Blue o
Lemon yellow
Na
Na®
Na
Na0oC.
CH3
H3C-
SO,Na
N=N
ÓH
NaogS
но-
Na
H,C
Figure 4.2 Structure formulas of three components in the food coloring mixture
Transcribed Image Text:MATERIALS Safety goggles pencil, ruler and scissors methanol chromatography paper plastic wash bottle ethanol 4 50ml graduated cylinder food coloring mixture 2-propanol 4 cork stoppers distilled water acetic acid 4 wire paper clips ethyl acetate 1 capillary tube cyclohexane PROCEDURE 1. Using a ruler; draw a straight pencil line across the chromatography paper, about 1.5cm from the bottom. 2. Use the capillary tube to put one small drop of dye on the pencil line. Let it dry. Repeat step 1-2 for other 3 trials with different developing solvents. 3. Fill each of four 50ml graduated cylinders with four different solvents you choose to about 5 ml. Use a cork stopper to suspend each filter paper strip in a graduated cylinder, as shown in Figure 4.1. The end of the filter paper should be below the solvent level; the dye spot should be above the solvent level. Permit the solvent in each graduated cylinder to rise up the filter paper until it is about 2cm from the top of 4. partices, (atoms or Tonst Remove the strips from the graduated cylinders. Using a pencil, mark on each strip the distance the solvent uncan u the paper. 5. has traveled from the point of origin. Record these distances as D; in a data table. 6. Measure on each paper strip the distance each dye spot has traveled. Record these distances as Dş. If the original dye spot has separated into several spots, measure and record the D, for each spot. Calculate the Rf value for each components in the dye for all trails. 7. Dispose and recycle materials according to teacher's instruction. Paper chp hooh Solvent front Figure 4.1 the apparatus with distill H2Q H-bonds With ethyl acetate: DDF & H-bm WEth Cyclohexane: LDF gwith 2-propanut: H-bonding. Solvent Allura Red YSI Brilliant Blue o Lemon yellow Na Na® Na Na0oC. CH3 H3C- SO,Na N=N ÓH NaogS но- Na H,C Figure 4.2 Structure formulas of three components in the food coloring mixture
metkanol
ethanol 2-prepanol
acetic
acid
acetate Cyclahoand
Transcribed Image Text:metkanol ethanol 2-prepanol acetic acid acetate Cyclahoand
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