C: 30.29%, H: 2.54%, other element: 67.17% 1213 LOD D 4000 10 Relative Intensity 100 80 8 40 20 0-titt 9 HPM-00-218 IS-NU-4404 25 5000 00 8 50 mpy 7 2000 75 6 T m/z HAVENUMBER! 5 100 ppm 1500 2H, d 4 ffffffm 125 W 3 1H, t N 150 1000 1 m 0 500 The J-values here are very small (2 Hz), indicating long-range coupling (more than 1 C away)

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.17QAP
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Solve the structure, label the peaks. 

C: 30.29%, H: 2.54%, other element: 67.17%
1213
LOD
D
4000
10
Relative Intensity
100
80
8
40
20
0-titt
9
HPM-00-218
IS-NU-4404
25
5000
00
8
50
mpy
7
2000
75
6
T
m/z
HAVENUMBER!
5
100
ppm
1500
2H, d
4
ffffffm
125
W
3
1H, t
N
150
1000
1
m
0
500
The J-values here
are very small
(2 Hz), indicating
long-range coupling
(more than 1 C
away)
Transcribed Image Text:C: 30.29%, H: 2.54%, other element: 67.17% 1213 LOD D 4000 10 Relative Intensity 100 80 8 40 20 0-titt 9 HPM-00-218 IS-NU-4404 25 5000 00 8 50 mpy 7 2000 75 6 T m/z HAVENUMBER! 5 100 ppm 1500 2H, d 4 ffffffm 125 W 3 1H, t N 150 1000 1 m 0 500 The J-values here are very small (2 Hz), indicating long-range coupling (more than 1 C away)
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