Can you please check my work for ochem prelab The lab is the preparation of an acetamide... we are using o-toluidine as the amine and acetic anhydride I've attached an image of my work...  For prelab we need the mass of the reactants, the limiting reagent, and the theoretical yield Thank you!

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Can you please check my work for ochem prelab

The lab is the preparation of an acetamide... we are using o-toluidine as the amine and acetic anhydride

I've attached an image of my work... 

For prelab we need the mass of the reactants, the limiting reagent, and the theoretical yield

Thank you!

Preparation of an Acetamide.
NH ₂
CH3
0-toluidine
+
Chemical Equation
O
CH3C N4NH₂+ (CH3CO) 20
acetic anhydride
o-toluidine
Acetic anhydride 1.4049
Theoretical Yield
-
ΝΗ
Mass of acetic anhydride 1.3mL | 1.08g = 1.404g
IML
Mass of o-toluidine
Limiting Reactant
N-phenylacetamide
1m² | 1.0049 = 1.004 g.
IML
CH3
Imol
102.099
CH3C6H4NHCOCH3 + CH300H
1.004g Imol
107.159
*0-toluidine is the limiting reactant
+
=
i
он
acetic acid
0.0138 mol
0.0094 mol
0.0094 mol 1 mol 135, 16g = 1.27 g of N-
1 mol
I mol
Phenyl acetamide
Transcribed Image Text:Preparation of an Acetamide. NH ₂ CH3 0-toluidine + Chemical Equation O CH3C N4NH₂+ (CH3CO) 20 acetic anhydride o-toluidine Acetic anhydride 1.4049 Theoretical Yield - ΝΗ Mass of acetic anhydride 1.3mL | 1.08g = 1.404g IML Mass of o-toluidine Limiting Reactant N-phenylacetamide 1m² | 1.0049 = 1.004 g. IML CH3 Imol 102.099 CH3C6H4NHCOCH3 + CH300H 1.004g Imol 107.159 *0-toluidine is the limiting reactant + = i он acetic acid 0.0138 mol 0.0094 mol 0.0094 mol 1 mol 135, 16g = 1.27 g of N- 1 mol I mol Phenyl acetamide
PROCEDURE:
1) Measure 1.0 mL (or 1.0 g, if a solid) of the amine into a tared 50 mL Erlenmeyer flask and
determine its mass.
2) Add 10 mL of water to the flask and swirl to mix.
3) Measure 1.3 mL of acetic anhydride into a tared container and determine its mass.
4) Using a Pasteur pipet, transfer the acetic anhydride to the aniline mixture in small portions.
Continue swirling during this addition.
Transcribed Image Text:PROCEDURE: 1) Measure 1.0 mL (or 1.0 g, if a solid) of the amine into a tared 50 mL Erlenmeyer flask and determine its mass. 2) Add 10 mL of water to the flask and swirl to mix. 3) Measure 1.3 mL of acetic anhydride into a tared container and determine its mass. 4) Using a Pasteur pipet, transfer the acetic anhydride to the aniline mixture in small portions. Continue swirling during this addition.
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