A continuous steady-state distillation column with a total condenser and a partial reboiler is separating 1-butanol from cyclohexanol at 1 atm. 1000 kmol/h of the said binary mixture consisting of 45 mol% 1-butanol is being fed to the column. It is desired to have a distillate product that is 95 mol% 1-butanol and a bottoms product that is 2 mol% 1-butanol. Assume CMO. The reflux ratio and the boil-up ratio are 1.30 and 1.80, respectively. a) Perform mass balances to plot the enriching section, stripping section, and the feed line. b) What type of feed is used in the column? c) Find number of ideal stages for desired separation and the optimal feed tray location.

Introduction to Chemical Engineering Thermodynamics
8th Edition
ISBN:9781259696527
Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Publisher:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Chapter1: Introduction
Section: Chapter Questions
Problem 1.1P
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A continuous steady-state distillation column with a total condenser and a partial reboiler is
separating 1-butanol from cyclohexanol at 1 atm. 1000 kmol/h of the said binary mixture
consisting of 45 mol% 1-butanol is being fed to the column. It is desired to have a distillate product
that is 95 mol% 1-butanol and a bottoms product that is 2 mol% 1-butanol. Assume CMO. The
reflux ratio and the boil-up ratio are 1.30 and 1.80, respectively.
a) Perform mass balances to plot the enriching section, stripping section, and the feed line.
b) What type of feed is used in the column?
c) Find number of ideal stages for desired separation and the optimal feed tray location.
d) Determine the concentration of the mixture at each stage.
e) Calculate the flowrates of the distillate and bottoms, as well as the reflux and boil-off.
f) Find the minimum number of stages required to achieve the desired separation.
g) Find the minimum reflux ratio.

 

If needed below is the graphs. 

Equilibrium Data for n-propyl acetate/n-propyl benzene:
y (n-propyl acetate), mol.frac.
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.0
0.1
yx Plot for n-propyl acetate/n-propyl benzene
0.2
0.3
0.4
0.5
0.6
0.7
x (n-propyl acetate), mol.frac.
0.8
0.9
1.0
Transcribed Image Text:Equilibrium Data for n-propyl acetate/n-propyl benzene: y (n-propyl acetate), mol.frac. 1.0 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0.0 0.0 0.1 yx Plot for n-propyl acetate/n-propyl benzene 0.2 0.3 0.4 0.5 0.6 0.7 x (n-propyl acetate), mol.frac. 0.8 0.9 1.0
Equilibrium Data for 1-butanol/Cyclohexanol:
y (1-butanol), mol.frac.
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.0
0.1
yx Plot for 1-butanol/Cyclohexanol
0.2
0.3
0.4
0.5
0.6
x (1-butanol), mol.frac.
0.7
0.8
0.9
1.0
Transcribed Image Text:Equilibrium Data for 1-butanol/Cyclohexanol: y (1-butanol), mol.frac. 1.0 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0.0 0.0 0.1 yx Plot for 1-butanol/Cyclohexanol 0.2 0.3 0.4 0.5 0.6 x (1-butanol), mol.frac. 0.7 0.8 0.9 1.0
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