A 20g mixture containing 95% (by weight) of A and 5% of B is recrystallized in toluene (b.p. 110°C). Solubilities in g/100 mL are given below. What amount of solvent is needed to obtain pure A and how much pure A will be recovered? Show all calculations and explain your answers. Hint: the goal of a recrystallization is gl keep ALL of the impurity dissolved at the low temperature. Knowing that, how much solvent is needed for this example?
A 20g mixture containing 95% (by weight) of A and 5% of B is recrystallized in toluene (b.p. 110°C). Solubilities in g/100 mL are given below. What amount of solvent is needed to obtain pure A and how much pure A will be recovered? Show all calculations and explain your answers. Hint: the goal of a recrystallization is gl keep ALL of the impurity dissolved at the low temperature. Knowing that, how much solvent is needed for this example?
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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A 20g mixture containing 95% (by weight) of A and 5% of B is recrystallized in toluene (b.p. 110°C). Solubilities in g/100 mL are given below. What amount of solvent is needed to obtain pure A and how much pure A will be recovered? Show all calculations and explain your answers. Hint: the goal of a recrystallization is gl keep ALL of the impurity dissolved at the low temperature. Knowing that, how much solvent is needed for this example?

Transcribed Image Text:8
ontaining 95% (by weight) of A and 5% of B is recrystallized in toluene (b.p. 1
Solubilities in g/100 mL are given below. What amount of solvent is needed to obtain pure A ar
much pure A will be recovered? Show all calculations and explain your answers. Hint: the goal o
recrystallization is to keep ALL of the impurity dissolved at the low temperature. Knowing that,
much solvent is needed for this example?
Temperature
Solubility (g/100 ml)
A
BI
20⁰
110
10.0 g
8.0g
Experimental
NOTE: You will need a data table for your solvent tests and also you will need to report your m.p
appearance, and % yield of compound. Read the experiment then organize your data tables.
Warning! You will be expected to think and plan before you act on this experiment very lit
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