4,4,5-Trimethyl-2-cyclohexen-1-one. Cyclization of the al- kylation product from run 11 gave the title enone, bp 60-65 °C (air bath, 0.15 mm): NMR ô 0.96 (d, 3 H, J = 6 Hz, CH3CH), 1.02, 1.15 (s, 3 H each (CH3),C), 5.90, 6.69 (d, 1 H each, J = 10 Hz, CH=CH); IR 1670. These spectral properties are consistent with the structure and in fair agreement with those reported by Flaugh et al.23 %3D

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Find and read the article published in the Journal of Organic Chemistry titled "A Silyl Enol Ether Variation of the Robinson Annulation" by John W. Huffman, Shailesh M. Potnis, and Amruthur V. Satish. 

Find the information on the H NMR spectra of molecule 4,4,5-trimethyl-2-cyclohexen-1-one. 

There are ___ resonances in the spectrum.

___ of the resonances are singlets

___ of the resonances are doublets

4,4,5-Trimethyl-2-cyclohexen-1-one. Cyclization of the al-
kylation product from run 11 gave the title enone, bp 60-65 °C
(air bath, 0.15 mm): NMR ô 0.96 (d, 3 H, J
1.02, 1.15 (s, 3 H each (CH3),C), 5.90, 6.69 (d, 1 H each, J = 10
Hz, CH=CH); IR 1670. These spectral properties are consistent
with the structure and in fair agreement with those reported by
Flaugh et al.23
= 6 Hz, CH3CH),
Transcribed Image Text:4,4,5-Trimethyl-2-cyclohexen-1-one. Cyclization of the al- kylation product from run 11 gave the title enone, bp 60-65 °C (air bath, 0.15 mm): NMR ô 0.96 (d, 3 H, J 1.02, 1.15 (s, 3 H each (CH3),C), 5.90, 6.69 (d, 1 H each, J = 10 Hz, CH=CH); IR 1670. These spectral properties are consistent with the structure and in fair agreement with those reported by Flaugh et al.23 = 6 Hz, CH3CH),
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