4. You'll purify your aspirin product via recrystallization before you can weigh it. The Merck Index indicates that at room temperature, 300 mL of water - but only 5 mL of ethanol - will dissolve 1 gram of aspirin. But the water solubility of aspirin increases with temperature. At 37°C, 1 gram will dissolve in 100 mL of water. Note you'll use a MIXTURE of ethanol and water to recrystallize your aspirin product. a) Why is it essential that you NOT allow the ethanol-water recrystallization mixture to reach a boil? b) And why is it important not to use too large a volume of ethanol in your recrystallization?

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4. You'll purify your aspirin product via recrystallization before you can weigh it. The Merck Index indicates that at room
temperature, 300 mL of water - but only 5 mL of ethanol - will dissolve 1 gram of aspirin. But the water solubility of
aspirin increases with temperature. At 37°C, 1 gram will dissolve in 100 mL of water. Note you'll use a MIXTURE of
ethanol and water to recrystallize your aspirin product.
a) Why is it essential that you NOT allow the ethanol-water recrystallization mixture to reach a boil?
b) And why is it important not to use too large a volume of ethanol in your recrystallization?
Transcribed Image Text:4. You'll purify your aspirin product via recrystallization before you can weigh it. The Merck Index indicates that at room temperature, 300 mL of water - but only 5 mL of ethanol - will dissolve 1 gram of aspirin. But the water solubility of aspirin increases with temperature. At 37°C, 1 gram will dissolve in 100 mL of water. Note you'll use a MIXTURE of ethanol and water to recrystallize your aspirin product. a) Why is it essential that you NOT allow the ethanol-water recrystallization mixture to reach a boil? b) And why is it important not to use too large a volume of ethanol in your recrystallization?
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