4. Imagine you performed the following extraction steps on a solution of salicylic acid and (R)-carvone inethyl acetate. Draw the structure of salicylic acid and (R)-carvone after each step and predict the layer(organic or aqueous) it will be found in.OHOHsalicylic acid(R)-carvonea. The solution of salicylic acid and (R)-carvone in ethyl acetate is washed with water.b. The organic layer from part a is washed with aqueous sodium hydroxide.c. The aqueous layer from part b is neutralized by adding sulfuric acid. Then it is extracted with ethylacetate.

Answered: Image /qna-images/answer/8d7d266f-1124-4602-af84-07f5cc3023fd.jpg

4. Imagine you performed the following extraction steps on a solution of salicylic acid and (R)-carvone in ethyl acetate. Draw the structure of salicylic acid and (R)-carvone after each step and predict the layer (organic or aqueous) it will be found in.

4. Imagine you performed the following extraction steps on a solution of salicylic acid and (R)-carvone in ethyl acetate. Draw the structure of salicylic acid and (R)-carvone after each step and predict the layer (organic or aqueous) it will be found in.

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

See similar textbooks

Related questions

Q: 18) A student was given a mixture of the following compounds. CO₂H After dissolving the mixture in…

Q: Based on the Material Safety Data Sheets (MSDS) for the compounds, which of the compounds in this…

A: To assess the level of hazard of the given…

Q: 2.1g of sample are dissolved in methylene chloride and the sample is extracted with an aqueous…

Q: The question is: Provide a method for separating a mixture of benzophenone and tributylamine which…

A: The mixture of Benzophenone and tributylamine in diethyl ether taken in a separating funnel then…

Q: Consider analysis of a mixture of saturated and unsaturated triacylglycerols (fish oil). Consider 3…

A: The structure of saturated and unsaturated fatty acids are shown with examples below:

Q: Which qualitative analysis test from this module can help distinguish between different kinds of…

Q: 1. A compound of molecular formula C5H₁00 forms a yellow precipitate with reagent and a yellow…

A: #1.(a): Given the molecular formula for the unknown compound is C5H10O Degree of unsaturation(DU) of…

Q: Discuss the “green” implications of using dichloromethane (methylene chloride) as your primary…

A: Green implications of using DCM as primary extraction solvent:By keeping in mind the 12 principles…

Q: Considering the stoichiometry of the reaction (balance the equation!), what is the net oxidation…

A: The objective of the question is to calculate the net oxidation state difference of the carbons in…

Q: Suppose you took your two compounds, dissolved them in tertbutyl methyl ether and then added them to…

A: We know that, carboxylic acids are reacted with the sodium bicarbonate to form the respective sodium…

Q: Use the following atomic weights and quantities to calculate the overall % yield of…

Q: How could you separate a mixture of ethanol, 1-pentanol and 1-octanol. Discuss the steps in your…

A: Fractional distillation is a type of distillation which involves the separation of miscible liquids.…

Q: What product would you obtain if you evaporated the water from the NaOH layer prior to acidifying…

A: Ether layer contains acetanilide (C6H5NHCOCH3) and p-tert-butylphenol (p-C4H9-C6H4OH). On the…

Q: It may be possible that some m-toluic acid may remain unreacted or may have formed from the…

Q: 1a: Write the overall reaction for our esterification reaction, and its mechanism. 1b: Using the…

Q: For each of the following mixtures, suggest a separation technique and explain a basis for your…

Q: 10. Write out the mechanism (intermediate/transition state) for this reaction. Indicate…

A: Markovnikoffs rule - in an addition reaction , the negative part of the addendum attaches itself to…

Q: You could extract caffeine from neutral organics by treatment with aqueous HCl (acid). Write the…

Q: 00 Draw structural formulas for the a,ß-unsaturated aldehyde or ketone and the lithium…

A: Gilman reagents are commonly prepared from organolithium or organomagnesium compounds by…

Q: You need to recrystallize compound A. You are given several solvents to choose from. Briefly…

A: Recrystallization is a technique used to purify solid organic compounds. It is based on the…

Q: How would you go about separating a mixture of 1-chloro-4-methylbenze and salicylic acid using…

Q: You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC)…

Q: Which of the following statements is correct with regards to paracetamol? Dichloromethane is a good…

A: Recrystallization is a commonly used purification technique for solids, including paracetamol. In…

Q: You have a separatory funnel that contains a solution of 2-chlorobenzoic acid and 4-methylaniline in…

A: This question is based on extraction of compounds from a given mixture.

Q: The oxidation of 3-pentanol to 3-pentanone was performed in the lab and an IR was taken of the…

A: IR spectroscopy is a technique that detects the presence of different functional groups present in…

Q: 10) Write an equation for the reaction of n-propyl magnesium chloride and butanal (Not 3-…

A: The given reaction involve the nucleophilic addition of Grignard reagent (n-propyl magnesium…

Q: Your employer hands you a heterogeneous mixture and asks you to isolate all of thehexane that you…

A: 1. **Filtration**: Begin with a simple filtration to remove the sand, as it is an insoluble solid.…

Question

4. Imagine you performed the following extraction steps on a solution of salicylic acid and (R)-carvone in
ethyl acetate. Draw the structure of salicylic acid and (R)-carvone after each step and predict the layer
(organic or aqueous) it will be found in.
OH
OH
salicylic acid
(R)-carvone
a. The solution of salicylic acid and (R)-carvone in ethyl acetate is washed with water.
b. The organic layer from part a is washed with aqueous sodium hydroxide.
c. The aqueous layer from part b is neutralized by adding sulfuric acid. Then it is extracted with ethyl
acetate.

Expert Solution

This question has been solved!

Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.

This is a popular solution!

SEE SOLUTION Check out a sample Q&A here

Step 1

VIEW

Step 2

VIEW

Trending now

This is a popular solution!

Step by step

Solved in 2 steps with 1 images

SEE SOLUTION Check out a sample Q&A here

Knowledge Booster

Sample Preparation in Analytical Chemistry

Learn more about

Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.

Similar questions

In the lab for the synthesis of methyl m-nitrobenzoate from methyl benzoate using HNO3 and H2SO4 via EAS, the product is recrystallized to remove impurities using 95% ethanol. Would o-nitrobenzoate and methyl p-nitrobenzoate be considered impurities? If that is so, how come ethanol can remove o-nitrobenzoate and methyl p-nitrobenzoate, but has no effect on m-nitrobenzoate? Thank you.
What change can be made to allow for a faster rate of reaction if poor solubility of KOH in ethanol slowed the rate and led to slow deprotonation of dibenzyl ketone?
Are there other tests that could be used to determine if cyclohexanol is present in your product? Give at least one test with some detail of what you would expect.
10) Dr. Rashmi uses a rather specific three-steps procedure (described below) to cook up a spicy sugar derivative. Why does she make use of such a protocol? Describe the purpose of each steps. 1) acetone, cat. H* 2) 2,5-dimethylbenzyl bromide, NaH 3) H30*, r.t. он NH2 "NH2 'Buo "Buo ´OBu O'Bu
Calculate The Theoretical Yield Of Alkenes For the acid catalyzed dehydration of 2-methyl-2-butanol Note: 20.0 ml of 2-methyl-2-butanol were used and 10 mL of concentrated sulfuric acid were used. Note the real amount produced was 10.92 g.
Could I please have help with number 5: Show the full structure of the salt that forms when triethylamine reacts with hydrochloric acid