4 Information: Each spectra below was obtained from a pure compound. Mass Spectrum parent peaks (M) are listed for all examples. IR peaks listed are strong (s) unless otherwise indicated for signals above 1500 cm³¹ ¹H NMR Spectra, the integral is given in number of hydrogens (#H) or as a relative ratio. Important coupling constants (J-values) are listed next to the peaks for some examples. For some spectra, an inset (grey box) is also given showing a "zoom-in" on an important part of the spectrum. Mass Spectrometry (not shown): [M] = 122 m/z -1 Infrared Spectroscopy (not shown): 3364, 3030, 2973, 1493, 1451, 1408, 1178 cm*¹ ¹H Nuclear Magnetic Resonance. 8 m 5H 13C Nuclear Magnetic Resonance. S 1H1H PPM 3 3H

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
icon
Concept explainers
Question

determine the chemical structure and name the structure.

**Spectral Analysis of a Pure Compound**

**Information**: Each spectrum below was obtained from a pure compound. The Mass Spectrum parent peaks (M) are listed for all examples. IR peaks listed are strong (s) unless otherwise indicated for signals above 1500 cm⁻¹. In ¹H NMR spectra, the integral is given in the number of hydrogens (H) or as a relative ratio. Important coupling constants (J-values) are listed next to the peaks for some examples. For some spectra, an inset (grey box) is also given showing a "zoom-in" on an important part of the spectrum.

### Mass Spectrometry (not shown):
- **[M] = 122 m/z**

### Infrared Spectroscopy (not shown):
- **Peaks:** 3364, 3030, 2973, 1493, 1451, 1408, 1178 cm⁻¹

### ¹H Nuclear Magnetic Resonance:
This spectrum displays several peaks at different parts per million (PPM). 

- A peak at approximately 7.2 PPM, labeled 'm', integrates for 5 protons (5H).
- A peak at around 5.0 PPM, labeled 'q', integrates for 1 proton (1H).
- A peak around 4.8 PPM, labeled 's', integrates for 1 proton (1H).
- A peak at about 1.2 PPM, labeled 'd', integrates for 3 protons (3H).

### ¹³C Nuclear Magnetic Resonance:
This spectrum shows multiple peaks indicating different carbon environments at various PPM values.

- Significant peaks are located around 150, 130, 120, 100, and 20 PPM, displaying the diverse electronic environments experienced by carbon atoms in the molecule.

These spectroscopic methods collectively provide insight into the structural features of the compound, including its mass, functional groups, and hydrogen and carbon environments.
Transcribed Image Text:**Spectral Analysis of a Pure Compound** **Information**: Each spectrum below was obtained from a pure compound. The Mass Spectrum parent peaks (M) are listed for all examples. IR peaks listed are strong (s) unless otherwise indicated for signals above 1500 cm⁻¹. In ¹H NMR spectra, the integral is given in the number of hydrogens (H) or as a relative ratio. Important coupling constants (J-values) are listed next to the peaks for some examples. For some spectra, an inset (grey box) is also given showing a "zoom-in" on an important part of the spectrum. ### Mass Spectrometry (not shown): - **[M] = 122 m/z** ### Infrared Spectroscopy (not shown): - **Peaks:** 3364, 3030, 2973, 1493, 1451, 1408, 1178 cm⁻¹ ### ¹H Nuclear Magnetic Resonance: This spectrum displays several peaks at different parts per million (PPM). - A peak at approximately 7.2 PPM, labeled 'm', integrates for 5 protons (5H). - A peak at around 5.0 PPM, labeled 'q', integrates for 1 proton (1H). - A peak around 4.8 PPM, labeled 's', integrates for 1 proton (1H). - A peak at about 1.2 PPM, labeled 'd', integrates for 3 protons (3H). ### ¹³C Nuclear Magnetic Resonance: This spectrum shows multiple peaks indicating different carbon environments at various PPM values. - Significant peaks are located around 150, 130, 120, 100, and 20 PPM, displaying the diverse electronic environments experienced by carbon atoms in the molecule. These spectroscopic methods collectively provide insight into the structural features of the compound, including its mass, functional groups, and hydrogen and carbon environments.
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 2 steps with 1 images

Blurred answer
Knowledge Booster
IR Spectroscopy of Organic Molecules
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY