Please correct answer and don't use hend raiting 24-3. (a) What are the advantages and disadvantages of using a nar-rower open tubular column?(b) What are the advantages and disadvantages of using a longeropen tubular column?(c) What are the advantages and disadvantages of using a thickerfilm of stationary phase?

(a) Advantages and Disadvantages of Using a Narrower Open Tubular ColumnAdvantages:Increased…

Answered: 24-3. (a) What are the advantages and…

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter25: Voltammetry

Section: Chapter Questions

Problem 25.11QAP

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In a moving boundary experiment with 0.1N KCI using 0.005N LICI, as indicator solution, a constant current of 0.005893 amp was passed for 2130 seconds and the boundary was observed to move through 5.6cm in a tube of 0.1142 sq.cm. .cross-section. Calculate the transport number of K+ and CI – ions .a t- = 0.492, t+ =0.508 t+ = 0.402, t- =0.598 .b O .c O t+ = 0.492, t- =0.508 .d O t+ = 0.402, t- =0.598
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6
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24-3. (a) What are the advantages and disadvantages of using a nar- rower open tubular column? (b) What are the advantages and disadvantages of using a longer open tubular column? (c) What are the advantages and disadvantages of using a thicker film of stationary phase?