2 3 4 6 7 8 100 QUESTION 4 How much sample should be loaded into the capillary tube for a Melting Range Determination? O Enough sample so that the solid is clearly visible under the magnifying lens, but not enough of a sample height to extend out of the heated range of the DigiMelt. O The tube should be filled all the way up. Only a sinige grain of solid can be added. This is often difficult to see under the magnifying lens. O The tube should be filled halfway up.
2 3 4 6 7 8 100 QUESTION 4 How much sample should be loaded into the capillary tube for a Melting Range Determination? O Enough sample so that the solid is clearly visible under the magnifying lens, but not enough of a sample height to extend out of the heated range of the DigiMelt. O The tube should be filled all the way up. Only a sinige grain of solid can be added. This is often difficult to see under the magnifying lens. O The tube should be filled halfway up.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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2 3
QUESTION 4
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How much sample should be loaded into the capillary tube for a Melting Range Determination?
O Enough sample so that the solid is clearly visible under the magnifying lens, but not enough of a sample height to extend out of the heated range of the DigiMelt.
O The tube should be filled all the way up.
S
O Only a sinige grain of solid can be added. This is often difficult to see under the magnifying lens.
O The tube should be filled halfway up.
6
QUESTION 5
You record the following melting ranges for your unknown, for known standards, and for mixed melting ranges:
Unknown #14: 78-80 °C.
QUESTION 6
Naphthalene: 78-80 °C
Vanillin: 78-80 °C
Mixed #14 with Napththalene: 66-75 °C
Mixed #14 with Vanillin: 78-80 °C
Which statement best summarizes unknown #14?
O Unknown #14 is already a mixture of naphthalene and vanillin.
O Unknown #14 may be vanillin, but not naphthalene.
O Unknown #14 may be vanillin or naphthalene.
O Unknown #14 may be naphthalene, but not vanillin.
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8
What properties describe a good solvent for a single-solvent recrystallization?
O Dissolves the solid when cold, but not when hot.
3
O Does not dissolve the solid at any temperature.
O Dissolves the solid whether hot or cold.
O Dissolves the solid when hot, but not when cold.
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