1. For the following compounds, determine the following: A. Number of peaks, B. Integral of each peak, C. Estimate of each peak location (ppm), D. Splitting pattern for each peak (singlet, doublet, triplet, etc.) For example, ethanol (CH3CH2OH) would be 3 peaks: CH3 peak at -1.5 ppm (3H, triplet), CH2 at -3.5 ppm (2H, quartet), and OH peak at -4.5 ppm (1H, singlet). This is dihydropyran, which is used as a "protecting group" for alcohols during organic synthesis. Protecting groups are chemical modifications that mask a functional group and prevent an undesired side reaction from occurring. This is a common reagent called "Boc anhydride" (like the sound a chicken makes - boc boc boc) and is used as a protecting group for amines during peptide synthesis. HO ΟΗ OH СОН This is the meso form of tartaric acid. Because it's a meso compound, this affects the number of peaks in its NMR spectrum.

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Chapter1: Chemical Foundations
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1. For the following compounds, determine the following:
A. Number of peaks,
B. Integral of each peak,
C. Estimate of each peak location (ppm),
D. Splitting pattern for each peak (singlet, doublet, triplet, etc.)
For example, ethanol (CH3CH2OH) would be 3 peaks: CH3 peak at -1.5 ppm (3H, triplet),
CH2 at -3.5 ppm (2H, quartet), and OH peak at -4.5 ppm (1H, singlet).
This is dihydropyran, which is used as a "protecting group" for alcohols during organic synthesis.
Protecting groups are chemical modifications that mask a functional group and prevent an
undesired side reaction from occurring.
This is a common reagent called "Boc anhydride" (like the sound a chicken makes - boc boc boc)
and is used as a protecting group for amines during peptide synthesis.
HO
ΟΗ
OH
СОН
This is the meso form of tartaric acid. Because it's a meso compound, this affects the number of
peaks in its NMR spectrum.
Transcribed Image Text:1. For the following compounds, determine the following: A. Number of peaks, B. Integral of each peak, C. Estimate of each peak location (ppm), D. Splitting pattern for each peak (singlet, doublet, triplet, etc.) For example, ethanol (CH3CH2OH) would be 3 peaks: CH3 peak at -1.5 ppm (3H, triplet), CH2 at -3.5 ppm (2H, quartet), and OH peak at -4.5 ppm (1H, singlet). This is dihydropyran, which is used as a "protecting group" for alcohols during organic synthesis. Protecting groups are chemical modifications that mask a functional group and prevent an undesired side reaction from occurring. This is a common reagent called "Boc anhydride" (like the sound a chicken makes - boc boc boc) and is used as a protecting group for amines during peptide synthesis. HO ΟΗ OH СОН This is the meso form of tartaric acid. Because it's a meso compound, this affects the number of peaks in its NMR spectrum.
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