0.56 g 1,4‐dimethoxybenzene, 0.9 mL 2‐chloro‐2‐methylpropane, 5 mL nitrobenzene and 0.52 g graphite were combined, and the mixture was refluxed for 1.5 hours. It was then cooled to room temperature and filtered. The filtered graphite was washed with 15 mL hexane. The filtrate was distilled under vacuum to remove any remaining 1,4‐dimethoxybenzene, 2‐chloro‐2‐ methylpropane and nitrobenzene (6.3 g), yielding 0.44 g 1,4‐di‐tert‐butyl‐2,5‐dimethoxybenzene (43.4% yield). What is the Atom economy, E factor, and effective mass yield?
0.56 g 1,4‐dimethoxybenzene, 0.9 mL 2‐chloro‐2‐methylpropane, 5 mL nitrobenzene and 0.52 g graphite were combined, and the mixture was refluxed for 1.5 hours. It was then cooled to room temperature and filtered. The filtered graphite was washed with 15 mL hexane. The filtrate was distilled under vacuum to remove any remaining 1,4‐dimethoxybenzene, 2‐chloro‐2‐ methylpropane and nitrobenzene (6.3 g), yielding 0.44 g 1,4‐di‐tert‐butyl‐2,5‐dimethoxybenzene (43.4% yield). What is the Atom economy, E factor, and effective mass yield?
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter23: Potentiometry
Section: Chapter Questions
Problem 23.12QAP: What arc the advantages of microfabricated ISEs? Describe typical applications of this type of...
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0.56 g 1,4‐dimethoxybenzene, 0.9 mL 2‐chloro‐2‐methylpropane, 5 mL nitrobenzene and 0.52 g graphite were combined, and the mixture was refluxed for 1.5 hours. It was then cooled to room temperature and filtered. The filtered graphite was washed with 15 mL hexane. The filtrate was distilled under vacuum to remove any remaining 1,4‐dimethoxybenzene, 2‐chloro‐2‐ methylpropane and nitrobenzene (6.3 g), yielding 0.44 g 1,4‐di‐tert‐butyl‐2,5‐dimethoxybenzene (43.4% yield). What is the Atom economy, E factor, and effective mass yield?
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