6_CaRedoxReport_Ella Keheley

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Texas A&M University *

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317

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Statistics

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Apr 3, 2024

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pdf

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3

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Lab Report 6 Volumetric Determination of %CaO using KMnO 4 Name: Ella Keheley Unknown #: 12 Date: 2/29/24 Standardization of KMnO 4 Solution ( by titration with standard Na 2 C 2 O 4 ) Trial # Mass of Na 2 C 2 O 4 (g) Titration Volume (mL of KMnO 4 ) Molarity ( M of KMnO 4 ) 1 0.2502 34.90 0.02140 2 0.2506 34.85 0.02147 3 0.2499 34.30 0.02175 4 0.2501 35.10 0.02139 Average = Standard Deviation = 0.02150 0.000169 Results -- Analysis of %CaO in Limestone Unknown Trial # Mass of unknown sample (g) Titration Volume (mL of KMnO 4 ) Mass Percent (% CaO) 1 0.2496 32.40 39.13 2 0.2508 33.90 40.74 3 0.2481 36.60 44.46 Average = Standard Deviation = 41.44 2.73 Calculations Molarity of KMnO 4 solution for Trial #1 of standardization 0.2502 𝑔 ?𝑎 2 𝐶 2 ? 4 × 1 ??? ?𝑎 2 𝐶 2 ? 4 134.00 𝑔 ?𝑎 2 𝐶 2 ? 4 × 2 ??? ???? 4 5 ??? ?𝑎 2 𝐶 2 ? 4 × 1 0.03490 ? ???? 4 = 0.02140 ? ???? 4 Mass Percent CaO for Trial # 1 0.03240 ? ???? 4 × 0.02150 ??? ???? 4 1 ? ???? 4 × 5 ??? 𝐶𝑎? 2 ??? ???? 4 × 56.077 𝑔 𝐶𝑎? 1 ??? 𝐶𝑎? = 0.09766 𝑔 𝐶𝑎? 0.09766 𝑔 0.2496 𝑔 × 100 = 39.13 % CaO Photo Documentation Photo of a representative endpoint from your standardization
Photo of a representative endpoint from your unknown analysis Conclusion: Describe how you managed your time most effectively in this experiment (limit to one paragraph). o Since this lab required heating many solutions, I prioritized anything that needed to reach a certain temperature first and then made other solutions, cleaning glassware, or measuring samples while waiting for solutions to heat up. What also helped in this procedure was talking through each step with a lab mate before starting to fully understand what all needed to be done and come up with a plan for each step to be most efficient. Let me know if anything unusual happened to affect your data; if the procedure went as expected, no need to comment. Raw Data Scan or photograph your data tables and insert below, making sure TA signatures are visible.
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