MACROSCALE+MICRO.ORG...-OWLV2 ACCESS
7th Edition
ISBN: 9781305884175
Author: Williamson
Publisher: CENGAGE L
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Chapter 9, Problem 5Q
Interpretation Introduction
Interpretation:
The reason for the separation of compounds as a mixture instead of individual components should be speculated.
Concept introduction:
A separation technique used for the segregation of components of chemical mixture based on the difference between the adsorption of different components in the stationary and mobile phase is called column chromatography.
It is used for purification or segregation of compounds. It consists of two phases namely:
- Stationary phase (solid)
- Mobile phase (generally liquid)
Silica gel is commonly used as the stationary phase.
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Part VII. Below are the 'HNMR, 13 C-NMR, COSY 2D- NMR, and HSQC 2D-NMR (similar with HETCOR but axes are reversed) spectra of an
organic compound with molecular formula C6H1003 - Assign chemical shift values to the H and c atoms of the
compound. Find the structure. Show complete solutions.
Predicted 1H NMR Spectrum
4.7 4.6 4.5 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 2.7 2.6 2.5 2.4 2.3 2.2 2.1 2.0 1.9 1.8 1.7 1.6 1.5 1.4 1.3 1.2 1.1
f1 (ppm)
Predicted 13C NMR Spectrum
100
f1 (ppm)
30
220 210 200 190 180
170
160 150 140 130 120
110
90
80
70
-26
60
50
40
46
30
20
115
10
1.0 0.9 0.8
0
-10
Q: Arrange BCC and Fec
metals, in sequence from the
Fable (Dr. R's slides) and
Calculate Volume and Density.
Aa
BCC
V
52 5
SFCC
None
Chapter 9 Solutions
MACROSCALE+MICRO.ORG...-OWLV2 ACCESS
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