(a) Interpretation: Preparation of N - phenylbenzamide from an amine and an acid chloride is to be predicted. Concept introduction: The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

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Answer 1

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Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

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Part 2. A solution of 6.00g of substance B in 100.0mL of aqueous solution is in equilibrium, at room temperature, wl a solution of B in diethyl ether (ethoxyethane) containing 25.0 g of B in 50.0 mL 9) what is the distribution coefficient of substance B b) what is the mass of B extracted by shaking 200 ml of an aqueous solution containing 10g of B with call at room temp): i) 100 mL of diethyl ether ii) 50ml of diethyl ether twice iii) 25ml of diethyl ether four times

- Rank the following groups of compounds from most acidic (1) to least acidic (4). Place the number corresponding to the compound's relative rank in the blank below the structure. a. NO₂ NO₂ CH2CH2CH2CH2OH CH3 CH3CH2CHOH CH3CH2CH2CH2OH NO₂ CH3CHCH2CH2OH b. OH OH CH₂OH CO₂H HC CN CN CN

Give the major organic product(s) of the following reactions or sequences of reactions. Show all relevant stereochemistry a. H MgBr 1. ether 2. H₂O* 4 COH b. 1. LIAIH, ether 2. H₂O Choose the best reagent(s) for carrying out the following conversions from the list provided below. Place the letter of the best choice in the blank to the left of the conversion. Reagents may be used more than once. a. 1. CH3MgBr, ether 2. H3O+ NaOH b. 1. PBr3 2. C. 2. 1. (CH3)3SiCl, (CH3CH2)3N CH3MgBr, ether 3. H₂O*+ 2. H3O+ e. 1. p-TosCl, pyridine f. نها g. 2. NaOH CrO3, H₂SO4, H₂O 1. NaBH4, ethanol 2. H30* h. PCC, CH2Cl2 Ovoldo-6 a. b. OH OH H OH O any organic

Answer 2

Question

Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

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Answer 3

Question

Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

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Answer 4

Question

Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

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Answer 5

Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Answer 6

Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Answer 7

Chapter 23, Problem 23.22P

Interpretation Introduction

(a)

Interpretation:

Preparation of N- phenylbenzamide from an amine and an acid chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann reaction. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Answer 8

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Answer 9

Interpretation Introduction

(b)

Interpretation:

Preparation of N- benzyl -N- ethylpropionamide from N- ethylaniline and a propionyl chloride is to be predicted.

Concept introduction:

The method used to synthesise amides from amines and acid chlorides in the presence of a base is known as Schotten Baumann. It is typically used to indicate two-phase solvent system in which one is water and other is an organic solvent. It is a condensation reaction in which two molecules combine to form a larger molecule.

Answer 10

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Answer 11

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Answer 12

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Answer 13

Ch. 23 - Prob. 23.1P Ch. 23 - Prob. 23.2P Ch. 23 - Prob. 23.3P Ch. 23 - Prob. 23.4P Ch. 23 - Prob. 23.5P Ch. 23 - Prob. 23.6P Ch. 23 - Prob. 23.7P Ch. 23 - Prob. 23.8P Ch. 23 - Prob. 23.9P Ch. 23 - Prob. 23.10P

Solution Summary: The author explains the Schotten Baumann reaction, which is used to synthesise amides from amines and acid chlorides in the presence of a base.

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Chapter 23 Solutions