Interpretation:
The method to identify a compound that is purified collected from a GC should be described.
Concept introduction:
Gas chromatography is efficiently used for the compounds that have high vapor pressures which allow them to pass through a GC column.
A gas chromatography does not identify compounds if unknown samples are loaded into the column. GC is one of type of partition chromatography, where the sample that has to be analyzed get adsorbed on the stationary phase.
The stationary phase is formed by high boiling nonvolatile liquid, usually a
The components of gas-liquid chromatography are as follows:
- High-pressure pure carrier gas source
- Flow controller
- Heated injection port
- Column and column oven
- Detector
- Recording device or data station

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Chapter 20 Solutions
LABORATORY TECHNIQUES IN ORGANIC CHEMIS
- If a reaction occurs, what would be the major products? Please include a detailed explanation as well as a drawing showing how the reaction occurs and what the final product is.arrow_forwardWould the following organic synthesis occur in one step? Add any missing products, required catalysts, inorganic reagents, and other important conditions. Please include a detailed explanation and drawings showing how the reaction may occur in one step.arrow_forward(a) Sketch the 'H NMR of the following chemical including the approximate chemical shifts, the multiplicity (splitting) of all signals and the integration (b) How many signals would you expect in the 13C NMR? CH3arrow_forward
- Draw the Show the major and minor product(s) for the following reaction mechanisms for both reactions and show all resonance structures for any Explain why the major product is favoured? intermediates H-Brarrow_forwardChoose the right answerarrow_forward8. What is the major product of the following reaction? KMnO4 b a TOH OH OH C d OH "OH HO OH OHarrow_forward
- Choose the right answerarrow_forward3. Draw ALL THE POSSBILE PRODUCTS AND THE MECHANISMS WITH ALL RESONANCE STRUCTURES. Explain using the resonance structures why the major product(s) are formed over the minor product(s). H₂SO4, HONO CHarrow_forward7. Provide the product(s), starting material(s) and/or condition(s) required for the No mechanisms required. below reaction HO + H-I CI FO Br2, FeBr3 O I-Oarrow_forward
- 6. Design the most efficient synthesis of the following product starting from phenot Provide the reaction conditions for each step (more than one step is required) and explain the selectivity of each reaction. NO MECHANISMS ARE REQUIRED. OH step(s) CIarrow_forwardWhat is the skeletal structure of the product of the following organic reaction?arrow_forwardIf a reaction occurs, what would be the major products? Please include a detailed explanation as well as a drawing showing how the reaction occurs and what the final product is.arrow_forward
- Chemical Principles in the LaboratoryChemistryISBN:9781305264434Author:Emil Slowinski, Wayne C. Wolsey, Robert RossiPublisher:Brooks Cole
