Laboratory Manual Chemistry in Context
8th Edition
ISBN: 9780073518121
Author: American Chemical Society
Publisher: McGraw-Hill Education
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Chapter 1.13, Problem 1.35CT
Interpretation Introduction
Interpretation:
Four factors which will bring the attention of citizens regarding air quality have to be given.
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Part VII. The H-NMR of a compound with molecular formula C5 H 10 O2 is given below.
Find the following:
(a) The no. of protons corresponding to each signal in the spectra
(6) Give the structure of the compound and assign the signals to each
proton in the compound.
a
70.2
Integration Values
C5H10O2
b
47.7
C
46.5
d
69.5
3.6 3.5
3.4 3.3 3.2 3.1 3.0
2.9 2.8
2.7
2.6 2.5
2.4 2.3 2.2 2.1 2.0
Chemical Shift (ppm)
1.9
1.8
1.7 1.6
1.5
1.4 1.3 1.2
1.1 1.0
0.9 0.8
Part 111. 1 H-NMR spectrum of a compound with integration values in red is given below.
Answer the following:
(a) write the signals in the 'H-NMR spectrum to the corresponding protons on the structure
of the molecule below.
(b) Identify the theoretical multiplicities for each proton in the compound. Also give the possible.
complex splitting patterns assuming J values are not similar.
там
Br
22
2
3
6
4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 5.2 5.0 4.8 4.6 4.4 4.2 4.0 3.8 3.6 3.4 3.2 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0
Chemical Shift (ppm)
ra.
Br
2
3
6
6
2.5
2.4
2.3
2.2
2.1
2.0
1.9
1.8
1.7
1.6
1.5
1.4
1.3
1.2
1.1
1.0
0.9
0.8
Chemical Shift (ppm)
2
2
Br
7.3
7.2
7.1
7.0 6.9
6.7 6.6 6.5
6.4
6.3
6.2
6.1
6.0
Chemical Shift (ppm)
5.9
5.8 5.7
5.5 5.4 5.3 5.2
5.0 4.9
1600°
1538°C
1493°C
In the diagram, the letter L indicates
that it is a liquid. Indicate its
components in the upper region
where only L is indicated.
The
iron-iron carbide phase
diagram.
Temperature (°C)
1400
8
1394°C
y+L
1200
2.14
y, Austenite
10000
912°C
800a
0.76
0.022
600
400
(Fe)
a, Ferrite
Composition (at% C)
15
1147°C
a + Fe3C
2
3
Composition (wt% C)
L
2500
4.30
2000
y + Fe3C
727°C
1500
Cementite (Fe3C)
1000
4
5
6
6.70
Temperature (°F)
Chapter 1 Solutions
Laboratory Manual Chemistry in Context
Ch. 1.1 - Prob. 1.2CTCh. 1.1 - The air is different in a pine forest, a bakery,...Ch. 1.1 - Scientific Practices More Oxygen ? We live in an...Ch. 1.2 - Prob. 1.5SCCh. 1.3 - Sulfur dioxide (SO2) is released in the air when...Ch. 1.4 - Prob. 1.9YTCh. 1.5 - Prob. 1.10CTCh. 1.6 - Prob. 1.11YTCh. 1.11 - Prob. 1.19YTCh. 1.11 - Prob. 1.21YT
Ch. 1.12 - Summarize what you have learned about ozone...Ch. 1.13 - Prob. 1.27YTCh. 1.13 - Prob. 1.28YTCh. 1.13 - Prob. 1.29SCCh. 1.13 - Prob. 1.30YTCh. 1.13 - Prob. 1.35CTCh. 1 - Prob. 1QCh. 1 - Prob. 2QCh. 1 - Prob. 3QCh. 1 - Identify three sources of particulate matter found...Ch. 1 - Prob. 5QCh. 1 - Prob. 6QCh. 1 - In these diagrams, two different types of atoms...Ch. 1 - Prob. 8QCh. 1 - Prob. 9QCh. 1 - Prob. 10QCh. 1 - Prob. 11QCh. 1 - Prob. 12QCh. 1 - Prob. 13QCh. 1 - Consider the following blank periodic table. a....Ch. 1 - Classify each of these substances as an element, a...Ch. 1 - Prob. 16QCh. 1 - Hydrocarbons are important fuels that we burn...Ch. 1 - Prob. 18QCh. 1 - Arrange these types of radiation in order of...Ch. 1 - These questions relate to the combustion of...Ch. 1 - Balance these equations in which ethane (C2 H4)...Ch. 1 - Prob. 22QCh. 1 - Count the atoms on both sides of the equation to...Ch. 1 - Prob. 24QCh. 1 - Nail polish remover containing acetone was spilled...Ch. 1 - Prob. 26QCh. 1 - Prob. 27QCh. 1 - Prob. 28QCh. 1 - Prob. 29QCh. 1 - Prob. 30QCh. 1 - A headline from the Anchorage Daily News in Alaska...Ch. 1 - Prob. 32QCh. 1 - Consider how life on Earth would change if the...Ch. 1 - Prob. 34QCh. 1 - Prob. 35QCh. 1 - Prob. 36QCh. 1 - Prob. 37QCh. 1 - Prob. 38QCh. 1 - Prob. 39QCh. 1 - Prob. 40QCh. 1 - Prob. 41QCh. 1 - Prob. 42QCh. 1 - Prob. 43QCh. 1 - Prob. 44QCh. 1 - Prob. 45QCh. 1 - Prob. 46QCh. 1 - Prob. 47QCh. 1 - Prob. 48QCh. 1 - Prob. 49QCh. 1 - Mercury, another serious air pollutant, is not...Ch. 1 - The EPA oversees the Presidential Green Chemistry...Ch. 1 - Prob. 52QCh. 1 - Here are two scanning electron micrograph images...Ch. 1 - Prob. 54QCh. 1 - Prob. 55QCh. 1 - Prob. 56QCh. 1 - Prob. 57QCh. 1 - You may have admired the beauty of hardwood...Ch. 1 - Prob. 59Q
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- Nonearrow_forwardPart II. Given below are the 'H-NMR spectrum at 300 MHz in CDC13 and mass spectrum using electron ionization of compound Brian. The FTIR of the said compound showed a strong peak at 1710 cm"). Determine the following: (a) molecular Formula and Degree of unsaturation of compound Brian (b) Basing on the given H-NMR spectrum tabulate the following (i) chemical shifts (ii) integration, ciii) multiplicity and (iv) interferences made for each signal (c) Draw the structure of compound Brian. ) ΕΙ 43 41 27 71 114 (M+) Hmmm 20 30 40 50 60 70 80 90 100 110 120 1H NMR spectrum 300 MHz in CDCl3 2.0 alle 1.0arrow_forwardThe iron-iron carbide phase diagram. In the diagram, the letter L indicates that it is a liquid. Indicate what its components are. Temperature (°C) 1600 10 Composition (at% C) 15 25 1538°C -1493°C 8 1400 1200 1394°C y+L L 2500 1147°C y. Austenite 2.14 4.30 2000 1000 912°C y + Fe3C 800ㅏ 0.76 0.022 600 a, Ferrite a + Fe3C 400 0 (Fe) Composition (wt% C) 727°C 1500 Cementite (Fe3C) 1000 6 6.70 Temperature (°F)arrow_forward
- Part V. Choose which isomer would give the 1H-NMR spectrum below. Justify your reasoning by assigning important signals to the Corresponding protons of the correct molecule. A D on of of of H H 88 2 90 7.8 7.6 7.4 80 5 6 [ppm] 7.2 6.8 6.6 6.4 ō [ppm]arrow_forwardShow work with explanation. don't give Ai generated solutionarrow_forwardQ7. a. Draw the line-bond structure of the major product for the following reaction, if a reaction occurs, assume monohalogenation. b. Calculate the product ratios using the following information (hint: use the number of hydrogens in each category present to calculate the ratios). Chlorination: 1° Reactivity=1 2° Reactivity=4 Heat + Cl2 3° Reactivity=5arrow_forward
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