Bundle: Chemistry For Today: General, Organic, And Biochemistry, 9th + Owlv2 With Mindtap Reader, 1 Term (6 Months) Printed Access Card
9th Edition
ISBN: 9781337580632
Author: Spencer L. Seager, Michael R. Slabaugh, Maren S. Hansen
Publisher: Cengage Learning
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Chapter 1, Problem 1.81E
Interpretation Introduction
Interpretation:
The Fahrenheit setting used for a baking temperature of
Concept introduction:
The conversion of a measurement from one unit to another is referred to as conversion of units. In a number, the digits which express the accurate measurement of the number are known as significant figures. It is counted starting from the first non-zero digit in the given number.
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(a
4 shows scanning electron microscope (SEM) images of extruded
actions of packing bed for two capillary columns of different diameters,
al 750 (bottom image) and b) 30-μm-i.d. Both columns are packed with the
same stationary phase, spherical particles with 1-um diameter.
A) When the columns were prepared, the figure shows that the column with
the larger diameter has more packing irregularities. Explain this observation.
B) Predict what affect this should have on band broadening and discuss your
prediction using the van Deemter terms.
C) Does this figure support your explanations in application question 33?
Explain why or why not and make any changes in your answers in light of
this figure.
Figure 4 SEM images of
sections of packed columns
for a) 750 and b) 30-um-i.d.
capillary columns.³
fcrip
= ↓ bandwidth Il temp
32. What impact (increase, decrease, or no change) does each of the following conditions have on the individual
components of the van Deemter equation and consequently, band broadening?
Increase temperature
Longer column
Using a gas mobile phase
instead of liquid
Smaller particle stationary phase
Multiple Paths
Diffusion
Mass Transfer
34. Figure 3 shows Van Deemter plots for a solute molecule using different column inner diameters (i.d.).
A) Predict whether decreasing the column inner diameters increase or decrease bandwidth.
B) Predict which van Deemter equation coefficient (A, B, or C) has the greatest effect on increasing or
decreasing bandwidth as a function of i.d. and justify your answer.
Figure 3 Van Deemter plots for hydroquinone using different column inner diameters (i.d. in μm). The data was
obtained from liquid chromatography experiments using fused-silica capillary columns packed with 1.0-μm particles.
35
20
H(um)
큰 20
15
90
0+
1500
100
75
550
01
02
594
05
μ(cm/sec)
30
15
10
Chapter 1 Solutions
Bundle: Chemistry For Today: General, Organic, And Biochemistry, 9th + Owlv2 With Mindtap Reader, 1 Term (6 Months) Printed Access Card
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Your...Ch. 1 - Prob. 1.83ECh. 1 - You have a 40-lb baggage limit for a transatlantic...Ch. 1 - You need 3.00lb of meat that sells for 3.41/lb...Ch. 1 - During a glucose tolerance test, the serum glucose...Ch. 1 - Prob. 1.87ECh. 1 - Prob. 1.88ECh. 1 - Prob. 1.89ECh. 1 - Prob. 1.90ECh. 1 - Prob. 1.91ECh. 1 - Immunoglobulin antibodies occur in five forms. A...Ch. 1 - Calculate the density of the following materials...Ch. 1 - Calculate the density of the following materials...Ch. 1 - Calculate the volume and density of a rectangular...Ch. 1 - Calculate the volume and density of a cube of lead...Ch. 1 - The volume of an irregularly shaped solid can be...Ch. 1 - The density of ether is 0.736g/mL. What is the...Ch. 1 - Calculate the mass in grams of 100.0mL of...Ch. 1 - Do the following metric system conversions by...Ch. 1 - A single water molecule has a mass of 2.991023g....Ch. 1 - Prob. 1.102ECh. 1 - Cooking oil has a density of 0.812g/mL. What is...Ch. 1 - Prob. 1.104ECh. 1 - At 4.0C, pure water has a density of 1.00g/mL. At...Ch. 1 - The following pairs of substances represent...Ch. 1 - Explain why a bathroom mirror becomes foggy when...Ch. 1 - Prob. 1.108ECh. 1 - Liquid mercury metal freezes to a solid at a...Ch. 1 - Prob. 1.110ECh. 1 - Show how the factor-unit method can be used to...Ch. 1 - Prob. 1.112ECh. 1 - Refer to Chemistry Around Us 1.2 and explain what...Ch. 1 - Prob. 1.114ECh. 1 - Which of the following properties is considered a...Ch. 1 - Which of the following properties depicts a...Ch. 1 - Which of the following is a mixture? a.sodium...Ch. 1 - Prob. 1.118ECh. 1 - Prob. 1.119ECh. 1 - The correct formula for converting Fahrenheit to...Ch. 1 - Prob. 1.121ECh. 1 - Prob. 1.122ECh. 1 - Prob. 1.123ECh. 1 - How many millimeters are there in one centimeter?...Ch. 1 - Convert 4.50102nm into pm. a.4.50102pm b.4.50102pm...Ch. 1 - Prob. 1.126ECh. 1 - Convert 4.50102nm into m. a.4.50102m b.4.501011m...Ch. 1 - The quantity 6185meters can be rewritten as: a....Ch. 1 - The number 1,000,000 is what power of 10? a. 106...Ch. 1 - What exponent or power of ten would you use to...Ch. 1 - Express 0.0562 in exponential notation. a....Ch. 1 - Write the correct answer correct number of...Ch. 1 - Prob. 1.133ECh. 1 - The percentage of oxygen by weight in Al2(SO4)3...Ch. 1 - Prob. 1.135ECh. 1 - The density of gold (Au) is 19.3g/cm3 and that of...
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