Homework Help is Here – Start Your Trial Now!
Science
Chemistry
You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid? 1. 2. 3. 4. Dry the solution in the beaker with sodium sulfate, filter, and evaporate off the solvent. Dissolve the crude solid ether and place in separatory funnel. Add 3M NaOH(aq) and shake and vent, then transfer ageous phase to a separate beaker. Repeat two times. Rinse the organic phase with brine and transfer to a beaker. Add 3M HCI(aq) and shake and vent, then transfer ageous phase to a separate flask. Repeat two times. To the combined aqueous extracts, add 6M HCI(aq) until the solution is acidic. To the combined aqueous extracts, add 6M NaOH(ag) until the solution is basic. Filter to collect the solid.

You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid? 1. 2. 3. 4. Dry the solution in the beaker with sodium sulfate, filter, and evaporate off the solvent. Dissolve the crude solid ether and place in separatory funnel. Add 3M NaOH(aq) and shake and vent, then transfer ageous phase to a separate beaker. Repeat two times. Rinse the organic phase with brine and transfer to a beaker. Add 3M HCI(aq) and shake and vent, then transfer ageous phase to a separate flask. Repeat two times. To the combined aqueous extracts, add 6M HCI(aq) until the solution is acidic. To the combined aqueous extracts, add 6M NaOH(ag) until the solution is basic. Filter to collect the solid.

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
See similar textbooks
icon
Related questions
Question

You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid?

You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid? 1. 2. 3. 4. Dry the solution in the beaker with sodium sulfate, filter, and evaporate off the solvent. Dissolve the crude solid in ether and place in separatory funnel. Add 3M NAOH(aq) and shake and vent, then transfer ageous phase to a separate beaker. Repeat two times. Rinse the organic phase with brine and transfer to a beaker. Add 3M HCI(aqg) and shake and vent, then transfer ageous phase to a separate flask. Repeat two times. To the combined aqueous extracts, add 6M HCI(aq) until the solution acidic. To the combined aqueous extracts, add 6M NaOH(ag) until the solution is basic. Filter to collect the solid.
Transcribed Image Text:You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid? 1. 2. 3. 4. Dry the solution in the beaker with sodium sulfate, filter, and evaporate off the solvent. Dissolve the crude solid in ether and place in separatory funnel. Add 3M NAOH(aq) and shake and vent, then transfer ageous phase to a separate beaker. Repeat two times. Rinse the organic phase with brine and transfer to a beaker. Add 3M HCI(aqg) and shake and vent, then transfer ageous phase to a separate flask. Repeat two times. To the combined aqueous extracts, add 6M HCI(aq) until the solution acidic. To the combined aqueous extracts, add 6M NaOH(ag) until the solution is basic. Filter to collect the solid.
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 2 steps

SEE SOLUTIONCheck out a sample Q&A here
Blurred answer
Knowledge Booster
Amines
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY
SEE MORE TEXTBOOKS