Wittig Reaction *PPH3 H. NANH2 H. + Br + NH, + NaBr PPH3 H. THE + Ph,PO Assign the characteristic signals on the following IR spectrum. 100 BIO-RAD 95 - 90 85 - 80 trans-Stilbene 75 70 65 60 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers Why did we need to exclude water from the reaction? What would happen if too much water was present? Why do we need to do a recrystallization after running the column chromatography? % Transmittance 2900 3025.1 -

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Wittig Reaction
*PPH3
PPH3
NANH2
H,
+ NH3 + NaBr
H.
+ Br
PPH3
H.
H.
THE
+ PH3PO
Assign the characteristic signals on the following IR spectrum.
100
BIO-RAD
95 -
90
85
80
trans-Stilbene
75
70
65
60
4000
3500
3000
2500
2000
1500
1000
500
Wavenumbers
Why did we need to exclude water from the reaction? What would happen if too
much water was present?
Why do we need to do a recrystallization after running the column chromatography?
% Transmittance
3082.4
1490.7
Transcribed Image Text:Wittig Reaction *PPH3 PPH3 NANH2 H, + NH3 + NaBr H. + Br PPH3 H. H. THE + PH3PO Assign the characteristic signals on the following IR spectrum. 100 BIO-RAD 95 - 90 85 80 trans-Stilbene 75 70 65 60 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers Why did we need to exclude water from the reaction? What would happen if too much water was present? Why do we need to do a recrystallization after running the column chromatography? % Transmittance 3082.4 1490.7
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