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what would the experimental yield be based on the data and please all of the numbers to get to the answer that is a percent. step by step

what would the experimental yield be based on the data and please all of the numbers to get to the answer that is a percent. step by step

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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what would the experimental yield be based on the data 

and please all of the numbers to get to the answer that is a percent.   step by step

Experiment 3: Williamson Ether Synthesis (Data sheet) Setup: 4.5 g of potassium hydroxide were dissolved in 8 mL of water in a 250 mL round-bottomed flask 2.55 g of p-cresol were added, and the mixture is swirled The pale-yellow mixture was brought to gentle reflux and a 6.70 mL of a 50 % aqueous solution (g/mL) of a-chloroacetic acid drop-wise using a separatory funnel Running the reaction: The mixture was refluxed for 10 minutes Product isolation: The hot mixture was transferred to a 100 mL beaker and 10 mL cold water was added Concentrated hydrochloric acid was added dropwise until pH<2. The yellowish mixture was placed in an ice bath for 20 minutes The mixture was filtered using a 5 cm a Büchner funnel using a vacuum filtration setup The crude product was recrystallized from 30 mL hot water After filtration, the solids were placed in a drying oven at 100 °C Product characterization: 2.30 g of a pale white solid М.p.: 137-140 °C
Transcribed Image Text:Experiment 3: Williamson Ether Synthesis (Data sheet) Setup: 4.5 g of potassium hydroxide were dissolved in 8 mL of water in a 250 mL round-bottomed flask 2.55 g of p-cresol were added, and the mixture is swirled The pale-yellow mixture was brought to gentle reflux and a 6.70 mL of a 50 % aqueous solution (g/mL) of a-chloroacetic acid drop-wise using a separatory funnel Running the reaction: The mixture was refluxed for 10 minutes Product isolation: The hot mixture was transferred to a 100 mL beaker and 10 mL cold water was added Concentrated hydrochloric acid was added dropwise until pH<2. The yellowish mixture was placed in an ice bath for 20 minutes The mixture was filtered using a 5 cm a Büchner funnel using a vacuum filtration setup The crude product was recrystallized from 30 mL hot water After filtration, the solids were placed in a drying oven at 100 °C Product characterization: 2.30 g of a pale white solid М.p.: 137-140 °C
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