Use the IR, MS and 13CNMR data provided to generate a reasonable structure for Unknown X. Make sure to explain your reasoning, label your structures and spectra thoroughly, and provide multiple pieces of evidence whenever possible.
Use the IR, MS and 13CNMR data provided to generate a reasonable structure for Unknown X. Make sure to explain your reasoning, label your structures and spectra thoroughly, and provide multiple pieces of evidence whenever possible.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
IR Spec, Mass Spec, and CNMR structure analysis.

Transcribed Image Text:Relative Intensity
LOD
100
o+
4000
80
Use the IR, MS and 13CNMR data provided to generate a reasonable structure for Unknown X.
Make sure to explain your reasoning, label your structures and spectra thoroughly, and provide
multiple pieces of evidence whenever possible.
83
20
0
25
3000
50
2000
75
100
m/z
HAVENUMBERI-
125
1970
1500
1000
162 164
150
175
500

Transcribed Image Text:13C NMR Spectrum
200
190
180 170
160
150
140
130
120
110
100
f1 (ppm)
90
80
70
60
-52.51
50
-38.02
40
-27.49
-25.64
30
20
10
0
-0.26
-0.24
-0.22
-0.20
-0.18
-0.16
-0.14
-0.12
-0.10
-0.08
-0.06
-0.04
-0.02
-0.00
--0.02
Expert Solution

Step 1
Given IR, mass and C NMR data for a compound.
To generate a reasonable structure for the unknown.
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