Use the IR, MS and 13CNMR data provided to generate a reasonable structure for Unknown X. Make sure to explain your reasoning, label your structures and spectra thoroughly, and provide multiple pieces of evidence whenever possible.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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IR Spec, Mass Spec, and CNMR structure analysis.

Relative Intensity
LOD
100
o+
4000
80
Use the IR, MS and 13CNMR data provided to generate a reasonable structure for Unknown X.
Make sure to explain your reasoning, label your structures and spectra thoroughly, and provide
multiple pieces of evidence whenever possible.
83
20
0
25
3000
50
2000
75
100
m/z
HAVENUMBERI-
125
1970
1500
1000
162 164
150
175
500
Transcribed Image Text:Relative Intensity LOD 100 o+ 4000 80 Use the IR, MS and 13CNMR data provided to generate a reasonable structure for Unknown X. Make sure to explain your reasoning, label your structures and spectra thoroughly, and provide multiple pieces of evidence whenever possible. 83 20 0 25 3000 50 2000 75 100 m/z HAVENUMBERI- 125 1970 1500 1000 162 164 150 175 500
13C NMR Spectrum
200
190
180 170
160
150
140
130
120
110
100
f1 (ppm)
90
80
70
60
-52.51
50
-38.02
40
-27.49
-25.64
30
20
10
0
-0.26
-0.24
-0.22
-0.20
-0.18
-0.16
-0.14
-0.12
-0.10
-0.08
-0.06
-0.04
-0.02
-0.00
--0.02
Transcribed Image Text:13C NMR Spectrum 200 190 180 170 160 150 140 130 120 110 100 f1 (ppm) 90 80 70 60 -52.51 50 -38.02 40 -27.49 -25.64 30 20 10 0 -0.26 -0.24 -0.22 -0.20 -0.18 -0.16 -0.14 -0.12 -0.10 -0.08 -0.06 -0.04 -0.02 -0.00 --0.02
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Given IR, mass and C NMR data for a compound.

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