Chapter16: Applications Of Neutralization Titrations
Section: Chapter Questions
Problem 16.32QAP
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Provide mechanism with curved arrows for
Part B: Synthesis of benzil
![Experiment 9B: Oxidation of Benzoin (Data Sheet)
Running the reaction:
• 2.50 g of benzoin and 0.39 g of tetrabutylammonium hydrogen sulfate were dissolved in
45 mL ethyl acetate in a 125 mL Erlenmeyer flask
19 mL of bleach, 10 m of water, and 9 mL of 0.05 M disodium hydrogenphosphate buffer
were added
• The flask was closed with parafilm and clamped
• The mixture was stirred vigorously for 60 minutes during which it turned bright yellow](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fe95435bc-a475-4a00-877d-f3d82e369349%2F92db8014-8f44-45c5-9b58-bb984608fe6b%2Fstko13j_processed.png&w=3840&q=75)
Transcribed Image Text:Experiment 9B: Oxidation of Benzoin (Data Sheet)
Running the reaction:
• 2.50 g of benzoin and 0.39 g of tetrabutylammonium hydrogen sulfate were dissolved in
45 mL ethyl acetate in a 125 mL Erlenmeyer flask
19 mL of bleach, 10 m of water, and 9 mL of 0.05 M disodium hydrogenphosphate buffer
were added
• The flask was closed with parafilm and clamped
• The mixture was stirred vigorously for 60 minutes during which it turned bright yellow
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