Please fill out the table II. Brady's Testanddinitrophenylhydrazine test (2,4-DNP). In this reaction, the carbonyl reacts with theamine of the hydrazine to give condensation product, called a hydrazone. The 2,4-DNP reagent gives an imine, and does not react with alcohols, carboxylic acids,amides, and esters.The wet product from part I may be used for Brady's Test. Obtain two test tubes,label one with "starting material" and the other "product." To each, add 100 mg ofthe corresponding test compound. Dissolve the solids in ethanol (0.5 mL or 10drops) by tapping the side of the test tube to agitate the mixture. To this solution,add 2,4-DNP reagent (1 mL or 20 drops) and mix. Let the mixture stand for 15 minand check for a red, yellow, or orange precipitate which is indicative of thehydrazone product. If no solids are observed, add deionized water (0.5 mL or 10drops), mix, and let stand for 5 min. Take note of your observations. Discard thesolutions in the labeled bottle in the fume hood.O₂Nسراسر2,4-DNPN—NH2R₁hydrazone ProcedureSubstanceMass (g)MW (g/mol)MmolEquivalentsIsoborneol6.5Oxone3.9NaCl1.8CamphorTheo.Part A. OxidationTo a 50 mL round bottomed flask equipped with a stir bar add isoborneol (6.5mmol). Add acetone (3 mL) and stir to dissolve the starting material. Add oxone (3.9mmol), followed by NaCl (1.8 mmol). Stir this heterogeneous solution vigorously.Add deionized water (1.5 mL) to the stirring solution and mix for 1 h.After the allotted time, add water (20 mL) and stir for 5 min to obtain a whitesuspension. Vacuum filter the material using a small Buchner funnel. Wash theproduct off the sides of the round bottomed flask with cold water (2 x 10 mL) anduse this to wash the filtrate. Place the Buchner funnel in a 100 mL beaker, cover thetop with a watch glass, and allow the wet product to dry in your drawer over theweek. Discard the filtrate in the aqueous waste container.Part B. SublimationWeigh the dry product in a 50 mL beaker. Cover the mouth of the beaker with awatch glass. Place the beaker on a heating plate. Place 1-2 cubes of ice on the watchglass. As the ice melts, pipette off excess water.021Slowly heat the beaker to sublime the camphor. Collect the sublimed crystals on aweighing paper by scraping the underside of the watch glass with a spatula. Weighthe crystals and obtain a melting point sample.Part C. CharacterizationI. IR SpectrumObtain the IR of the starting material and of the sublimed product. Note thetransformation in the functional group region of the spectrum. Rinse a pair of IR saltplates using dichloromethane. Hold the plate on its edge only. Using the tip of aspatula, place a small amount of the product on the face of one NaCl plate and add adrop of dichloromethane. Place the other one on top of it to make a sandwich. Youshould see a continuous film in between the salt plates. If not, open the sandwichand add one drop of dichloromethane, and make the sandwich. Follow instructionsfor obtaining an IR spectrum. Rinse off the NaCl plates which dichloromethane whenyou finish.

The given reaction is the reaction between isoborneol and oxone in the presence of NaCl to form…

Answered: Procedure Substance Mass (g) MW (g/mol)…

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Chemistry

Procedure Substance Mass (g) MW (g/mol) Mmol Equivalents Isoborneol 6.5 Oxone 3.9 NaCl 1.8 Camphor Theo.

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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In an alien world, a different periodic table exists. It is organized similar to the periodic table in our world, just smaller. The first group contains the alkali metals, the second group the alkaline earth metals, there are a few transition metals, and then some non-metals. The periodic table is shown below in picture form, and a table is given with molar masses and common ionic charges. Also in the table is a list of common ion groups (similar to carbonate, nitrate, etc. in our world.) Below is a table showing the molar masses and common ionic charges Element Symbol Atomic Number Atomic Mass Common Charge(s) FixedOrVariable Element or Group Name of anion Hydrogen H 0 Jellium J 1 1.28 2 Fixed Element Dogium D 2 2.48 -3 Fixed Element Dogide Gorillium G 3 4.87 -2 Fixed Element Gorillide Monkium M 4 7.27 -1 Fixed Element Monkide Jucium Oj 5 9.39 1 Fixed Element Racium R 6 11.18 2 Fixed Element Romium Ro 7 14.05 -3 Fixed Element Romide Julietium Ju…
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