Procedure of experimental   Test for carbonate ion (CO32-) Add 1 mL of 1M Na2CO3 (or your unknown) and 1 mL of 6M HCl to a small test tube.   C.      Test for sulfate ion (SO42-) Add 1 mL of 0.5 M Na2SO4 (or your unknown) and 1 mL of 6 M HCl to a small test tube. Next add a few drops of 1 M BaCl2.   D.     Test for phosphate ion (PO4 3-) Add 1 mL of 0.5 M Na2HPO4 (or your unknown) and 1 mL of 6 M HNO3 to a small test tube. Next add a 1 mL of 0.5 M (NH4)2MoO4 and stir thoroughly. Place the test tube in the hot water bath and continue to stir.   E.      Test for thiocyanate ion, (SCN-) Add 1 mL of 0.5 M KSCN (or your unknown) and 1 mL of 6 M acetic acid (HC2H3O2) to a small test tube. Now add 2 drops of 0.1 M Fe (NO3)3. A dark red solution indicates the presence of SCN-.   F.       Test for chloride ion, (Cl2-) Add 1 mL of 0.5 M NaCl (or your unknown) and 1 mL of 6 M HNO3 to a small test tube. Next add 2 to 3 drops of 0.1 M AgNO3.   G.     Test for nitrate ion, (NO3 –) Add 1 mL of 0.5 M NaNO3 (or your unknown) and 1 mL of 6 M NaOH to a small test tube. Then add a few granules of aluminum metal and put the test tube in the hot water bath. Place a red litmus paper directly above the test tube.   Complete the table.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Procedure of experimental

 

  1. Test for carbonate ion (CO32-)

Add 1 mL of 1M Na2CO3 (or your unknown) and 1 mL of 6M HCl to a small test tube.

 

C.      Test for sulfate ion (SO42-)

Add 1 mL of 0.5 M Na2SO4 (or your unknown) and 1 mL of 6 M HCl to a small test tube. Next add a few drops of 1 M BaCl2.

 

D.     Test for phosphate ion (PO4 3-)

Add 1 mL of 0.5 M Na2HPO4 (or your unknown) and 1 mL of 6 M HNO3 to a small test tube. Next add a 1 mL of 0.5 M (NH4)2MoO4 and stir thoroughly. Place the test tube in the hot water bath and continue to stir.

 

E.      Test for thiocyanate ion, (SCN-)

Add 1 mL of 0.5 M KSCN (or your unknown) and 1 mL of 6 M acetic acid (HC2H3O2) to a small test tube. Now add 2 drops of 0.1 M Fe (NO3)3. A dark red solution indicates the presence of SCN-.

 

F.       Test for chloride ion, (Cl2-)

Add 1 mL of 0.5 M NaCl (or your unknown) and 1 mL of 6 M HNO3 to a small test tube. Next add 2 to 3 drops of 0.1 M AgNO3.

 

G.     Test for nitrate ion, (NO3 –)

Add 1 mL of 0.5 M NaNO3 (or your unknown) and 1 mL of 6 M NaOH to a small test tube. Then add a few granules of aluminum metal and put the test tube in the hot water bath. Place a red litmus paper directly above the test tube.

 

Complete the table.

 

Experiment No. 11
QUALITATIVE ANALYSIS OF ANIONS
Table 1. Experimental Data
田
Anions
Experimental Results
Theoretical Results
so.-
PO,
SCN-
Clz-
NO,
Transcribed Image Text:Experiment No. 11 QUALITATIVE ANALYSIS OF ANIONS Table 1. Experimental Data 田 Anions Experimental Results Theoretical Results so.- PO, SCN- Clz- NO,
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