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Pho OBn HO HO OH HO a, b ACO OAC AcO HOA OPMP ACO- -OPMP OH 5 OAC 2 Scheme 1: Reagents: (a) acetic anhydride, sulfamic acid, 60 °C, 30 min, 91%; (b) Et3SiH, 12, 0-5 °C, 30 min, 82%.

Pho OBn HO HO OH HO a, b ACO OAC AcO HOA OPMP ACO- -OPMP OH 5 OAC 2 Scheme 1: Reagents: (a) acetic anhydride, sulfamic acid, 60 °C, 30 min, 91%; (b) Et3SiH, 12, 0-5 °C, 30 min, 82%.

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Scheme 1: Reagents: (a) acetic anhydride, sulfamic acid, 60°C,30min,91%; (b) Et3SiH,I2,0-5°C,30min,82%. 1) Draw the FULL, ARROW-PUSHING MECHANISM 2) Provide a verbalization of the mechanism for your reaction mechanism 3) What is happening at each step? What atom is nucleophilic? Which atom is electrophilic? Which bonds are made? Which bonds are broken? 4) Imagine you are trying to describe the reaction mechanism and I can't see your display - how would you describe the mechanism in a way that I know, that you know, what you are talking about. 

Pho OBn HO HO OH HO a, b ACO OAC AcO HOA OPMP ACO- -OPMP OH 5 OAC 2 Scheme 1: Reagents: (a) acetic anhydride, sulfamic acid, 60 °C, 30 min, 91%; (b) Et3SiH, 12, 0-5 °C, 30 min, 82%.
Transcribed Image Text:Pho OBn HO HO OH HO a, b ACO OAC AcO HOA OPMP ACO- -OPMP OH 5 OAC 2 Scheme 1: Reagents: (a) acetic anhydride, sulfamic acid, 60 °C, 30 min, 91%; (b) Et3SiH, 12, 0-5 °C, 30 min, 82%.
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