OMe1.2.1.0so, TBHP, H,O/THF2 TSОН, асetone, PhH, heat3. AICI,, CH,COCI, CH,C,3.1. BzOOBz, NBS, CCI42. Mg, THF; then Pd°L, PhBr3. HNO, H,SO,4. Zn, HCIBrMeoMeoMe5.MeMeo6.1. PdL. EtgN, MECNHOMe2. NABH, MEOHCI , ETGN, CH2CI2HO3.MeO.7.MeoHNMeNBrMe

1. Heck coupling followed Simmon Smith reaction. 2. Osmylation. Acetonide protection. Fridel craft…

OMe 1. 2. 1.Oso, TBHP, H,O/THF 2. TSOH, acetone, PhH, heat 3. AICI,, CH,COCI, CH,Cl2 3. 1. BZOOBZ, NBSs, CCL 2. Mg, THF; then Pd°L, PhBr 3. HNO, H,SO, 4. Zn, HCI 4. lan Br Meo Meo Me 5. Me Meo 6. OH 1. PdL. EtgN, MECN Me 2. NABH, MEOH CI, EtN, CH-Cl2 HO" 3. Me 7. Meo HN MeN Br Me

OMe 1. 2. 1.Oso, TBHP, H,O/THF 2. TSOH, acetone, PhH, heat 3. AICI,, CH,COCI, CH,Cl2 3. 1. BZOOBZ, NBSs, CCL 2. Mg, THF; then Pd°L, PhBr 3. HNO, H,SO, 4. Zn, HCI 4. lan Br Meo Meo Me 5. Me Meo 6. OH 1. PdL. EtgN, MECN Me 2. NABH, MEOH CI, EtN, CH-Cl2 HO" 3. Me 7. Meo HN MeN Br Me

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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Question

OMe
1.
2.
1.0so, TBHP, H,O/THF
2 TSОН, асetone, PhH, heat
3. AICI,, CH,COCI, CH,C,
3.
1. BzOOBz, NBS, CCI4
2. Mg, THF; then Pd°L, PhBr
3. HNO, H,SO,
4. Zn, HCI
Br
Meo
Meo
Me
5.
Me
Meo
6.
1. PdL. EtgN, MECN
HO
Me
2. NABH, MEOH
CI , ETGN, CH2CI2
HO
3.
Me
O.
7.
Meo
HN
MeN
Br
Me

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