May I please get some help with 13C NMR for C6H10O I need help with tabulating chemical shifts, splitting, neighboring protons, integration, fragments. Are there any special features?

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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May I please get some help with 13C NMR for C6H10O I need help with tabulating chemical shifts, splitting, neighboring protons, integration, fragments. Are there any special features?
**Title: Understanding the 13C NMR Spectrum of Unknown Compound #4**

**Introduction**

This document presents the 13C Nuclear Magnetic Resonance (NMR) spectrum for a compound labeled as "Unknown #4". NMR spectroscopy is a powerful tool used to identify the structure of organic compounds by analyzing the magnetic properties of carbon atoms.

**Graph Explanation**

The graph displayed is a 13C NMR spectrum featuring several peaks along the x-axis, which represents the chemical shift in parts per million (ppm). The scale ranges from approximately 0 to 210 ppm. The y-axis represents the intensity of the signals, indicating the presence of different carbon environments within the compound.

**Peak Analysis**

- Significant peaks are observed at the following chemical shifts, suggesting specific carbon environments in the compound:
  - Near 14 ppm
  - Around 30 ppm
  - Close to 70 ppm
  - Approximately 125-140 ppm
  - About 180 ppm

**Data Table**

A table is included with specific numerical values, likely denoting chemical shifts, multiplicity, and coupling constants. The table might list the observed peaks or additional spectral data for analysis.

- **SS:** 28, 3333
- **SF:** 25, 975 (others: 125, 941)
- **Other rows include various numerical entries likely used for internal referencing and detailed calculations.**

**Conclusion**

This spectrum provides a basis for deducing the structure of Unknown Compound #4 through the interpretation of chemical shifts and the identification of carbon atom types, such as alkyl, alkene, or carbonyl carbons. Further analysis and comparison with known data can help in structurally elucidating and confirming the identity of the compound.
Transcribed Image Text:**Title: Understanding the 13C NMR Spectrum of Unknown Compound #4** **Introduction** This document presents the 13C Nuclear Magnetic Resonance (NMR) spectrum for a compound labeled as "Unknown #4". NMR spectroscopy is a powerful tool used to identify the structure of organic compounds by analyzing the magnetic properties of carbon atoms. **Graph Explanation** The graph displayed is a 13C NMR spectrum featuring several peaks along the x-axis, which represents the chemical shift in parts per million (ppm). The scale ranges from approximately 0 to 210 ppm. The y-axis represents the intensity of the signals, indicating the presence of different carbon environments within the compound. **Peak Analysis** - Significant peaks are observed at the following chemical shifts, suggesting specific carbon environments in the compound: - Near 14 ppm - Around 30 ppm - Close to 70 ppm - Approximately 125-140 ppm - About 180 ppm **Data Table** A table is included with specific numerical values, likely denoting chemical shifts, multiplicity, and coupling constants. The table might list the observed peaks or additional spectral data for analysis. - **SS:** 28, 3333 - **SF:** 25, 975 (others: 125, 941) - **Other rows include various numerical entries likely used for internal referencing and detailed calculations.** **Conclusion** This spectrum provides a basis for deducing the structure of Unknown Compound #4 through the interpretation of chemical shifts and the identification of carbon atom types, such as alkyl, alkene, or carbonyl carbons. Further analysis and comparison with known data can help in structurally elucidating and confirming the identity of the compound.
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