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Science

Chemistry

mass

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter3: Stoichiometry

Section: Chapter Questions

Problem 45E: The mass spectrum of bromine (Br2) consists of three peaks with the following characteristics: Mass...

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When is sieving and fractional distillation a good method for separating mixtures? Cite an example.
You have a 11.5 mg sample of blood that contains various proteins. Hemoglobin is the only protein in the sample containing Fe. Hemoglobin contains 3.83% by mass of a compound called heme (C34H32FEN.O4, MW = 616.49 g/mol). You find that your 11.5 mg blood sample contains 10.9 micrograms of Fe. What is the mass percent of hemoglobin in your protein sample?
Which of the following statements are false for the time-of-flight mass spectrometer ? Light fragments travel faster than heavier fragments. A strong electric field is present in the tube by positioning a high-voltage metal grid in the path. Uses a magnetic field. Fragments are separated based on how fast they move through a drift tube. Signal is measured versus time, and then translated to a mass spectrum.
student found a bottle of unknown origin in the basement of an "CAUTION—contains С₁H₁O.” No other A old house. The bottle was labelled information was given, but inside the bottle were some white crystals. The student took the bottle to a chemistry laboratory, where she analyzed the crystals with the help of the laboratory staff. C₁2H₁6O reacted with Br₂ in CCl4 adding one mole of Br, and forming C₁₂H₁OB2₂. When a sample of C₁₂H₂O was reacted with O3 followed by Zn/H₂O, two different samples, J and K, were obtained. Compound J had a molecular formula of C.HgO₂, and its NMR is shown below. Compound K had a molecular formula of C₂H₂O, and it could be oxidized to compound L, with a molecular formula of C₂H₂O₂. The IR spectrum of L showed a very wide, strong band centred around 3000 cm*¹. The NMR spectrum of L showed only two different absorptions: a doublet (6H) at 0.9 ppm and a septet (1H) at 3.6 ppm. There was also a singlet (1H) off the scale at 11.8 ppm. students, deduce possible…
You have a 11.5 mg sample of blood that contains various proteins. Hemoglobin is the only protein in the sample containing Fe. Hemoglobin contains 3.83% by mass of a compound called heme (C₃₄H₃₂FeN₄O₄, MW = 616.49 g/mol). You find that your 11.5 mg blood sample contains 34.9 micrograms of Fe. What is the mass percent of hemoglobin in your protein sample? -don't prematureley round
A typical sports drink comes in a 20 fluid ounce bottle. 1 fluid ounce is 29.57 mL. Given your observed dye concentration, if you drank one bottle of sports drink per day for a year, how many grams of dye would you consume?
4. Two engineers are serving as trainees in a laboratory of a pharmaceutical company. One of their tasks involves determining the identity of a vitamin they were given by using any equipment or method at their disposal. As a hint, their supervisor gave them a list of possible candidates for the vitamins identity which includes: Vitamin Molecular Formula Folinic Acid C20 H23 N707 C3H11NO3 C,H,N20 C17H20N406 Pyridoxine Niacinamide Riboflavin To identify the vitamins identity, the two trainees separated their sample into two equal portions and performed two separate tests: [a.] Engr. Mayo used the flame atomic absorption spectrophotometer in order to identify the elemental composition of the sample which happens to be 59.0% C, 5.0% H and 22.9% N by mass [b.] Engr. Busog on the other hand mixed his 3.88 g sample with 30.0 mL of nitrobenzene, C,H5NO2 (Latent Heat of Fusion = 79.81 J/g). Using Beckmann's method, he determined the freezing point depression to be 7.1 deg C. Based on the tests…
18.
Which practice is NOT used to gauge accuracy? raw data and results from calibration checks B. fortification recoveries (c quality control samples blank samples E sample replications
14. Shown below are the mass spectra (without data tables) of four molecules. (The structure of each molecule is shown on the spectrum.) Mark the [M] peak for each, and indicate the molecular weight of the molecule. Relative Intensity Relative Intensity 100 80 60 40- 20 0-mm 10 100- 80 a. 20- 115-14-5501 0-mm 10 20 b. =0 20 30 30 40 40 50 50 60 m/z 60 m/z 70 70 80 80 90 100 90 100 Relative Intensity Relative Intensity 100- 80 40 20 0 100 80 40 10 20- 15-NU-5580 15 20 25 115--555 ont 10 20 30 30 35 40 45 50 55 m/z 40 50 m/z 60 60 70 65 70 75 80 Based on the five mass spectra you have seen, describe how one might identify the [M]* peak (molecular ion peak) on the mass spectrum of an unknown compound.
3. A student obtains a liquid sample of green food coloring that is known to contain a mixture of two solid pigments, one blue and one yellow, dissolved in an aqueous solution of ethanol. Which of the following setups is most appropriate for the student to use in order to separate and collect a substantial sample of each of the two pigments? In A. D. bab
What is polarity and how is polarity related to how chromatography works?