Mass Spectrum (not shown): M = 165 (100%) IR Spectrum (not shown): 3330, 3080, 2982, 1600, 1510 cm³¹ 1H NMR Spectrum d d S S 6 br s PPM 2H 2H 1H 4H 2H 13C NMR Spectrum (proton-decoupled) C FO CH 0 CH CH2 CH 160 140 120 100 80 PPM 60 60 40 20 0

Mass Spectrum (not shown): M = 165 (100%) IR Spectrum (not shown): 3330, 3080, 2982, 1600, 1510 cm³¹ 1H NMR Spectrum d d S S 6 br s PPM 2H 2H 1H 4H 2H 13C NMR Spectrum (proton-decoupled) C FO CH 0 CH CH2 CH 160 140 120 100 80 PPM 60 60 40 20 0

Organic Chemistry

9th Edition

ISBN:9781305080485

Author:John E. McMurry

Publisher:John E. McMurry

Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy

Section13.3: The Chemical Shift

Problem 4P: The following 1H NMR peaks were recorded on a spectrometer operating at 200 MHz. Convert each into...

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Question

Provide the unknown for the given data.

Mass Spectrum (not shown): M = 165 (100%)
IR Spectrum (not shown): 3330, 3080, 2982, 1600, 1510 cm³¹
1H NMR Spectrum
d
d
S
S
6
br s
PPM
2H
2H
1H
4H 2H
13C NMR Spectrum (proton-decoupled)
C
FO
CH
0
CH
CH2
CH
160
140
120
100
80
PPM
60
60
40
20
0

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