REACTION1. Using a burette, measure the cyclohexene (6.0 mmol) and transfer toa 125 mL erlenmeyer, along with acetone ([Cyclohexene] = 1 M). Adda stirbar.2. Cool the solution in an ice-bath for 10 minutes with magnetic stirring.3. Meanwhile, in a 2nd 125 mL erlenmeyer, dissolve Oxone (15.6 mmol) indeionized water ([Oxone] = 0.60 M).4. Attach a ring-clamp right over your flask. Add a closed separatoryfunnel, such that the bottom tip is partially inserted in the flask.5. Add your Oxone solution into the separatory funnel.6. When your cyclohexene solution is sufficiently cold, gently open thebottom valve of the separatory funnel to add the Oxone solution.Adjust the valve to obtain a flow of approximately 1–2 drops/second.7. Once the addition is complete, rinse the sepamillilitres of water.ory funnel with a few8. Remove the flask from the ice bath, and allow the reaction to stir atroom temperature for 20 minutes.9. After 20 minutes, add 12.5 M HCI (14.9 mmol) dropwise to the stirringsolution. Allow the reaction to stir for 10 minutes before proceedingwith liquid-liquid extraction (p.8).PURIFICATION– LIQUID-LIQUID EXTRACTION1. Assess the success of your reaction by performing a TLC on your crude reaction mixture. (See TLCprotocol below for details)2. Pour your resulting reaction mixture into 30 mL of water in a separatory funnel.3. Add 5 mL of ethyl acetate, and shake vigorously.|4. Drain the aqueous and organic layers into separate erlenmeyer flasks.5. Return the aqueous layer to the separatory funnel. Extract it two more times with additional 5 mL portionsof ethyl acetate, mixing well.|6. Drain the final aqueous layer. Add all of the organic fractions back into the separatory funnel.7. Wash the combined organic phase by adding 5 mL of clean water to the separatory funnel and mixing well.8. Drain both layers separately into their respective erlenmeyers.9. Analyze the purified organic extract by TLC using the protocol below.9) Liquid-liquid extraction is used here to purify the mixture obtained at the end of thereaction. For your respective reactionthe different species potentially found in solution at the end of the reaction to partitionbetween the organic and aqueous layers during the liquid-liquid extraction step? Explainyour prediction.Oxone), how you would expect

Liquid Liquid extraction is a technique of separating components of mixture using two immiscible…

Liquid-liquid extraction is used here to purify the mixture obtained at the end of the reaction. For your respective reaction the different species potentially found in solution at the end of the reaction to partition between the organic and aqueous layers during the liquid-liquid extraction step? Explain your prediction. Oxone), how you would expect

Liquid-liquid extraction is used here to purify the mixture obtained at the end of the reaction. For your respective reaction the different species potentially found in solution at the end of the reaction to partition between the organic and aqueous layers during the liquid-liquid extraction step? Explain your prediction. Oxone), how you would expect

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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