Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter32: Radiochemical Methods
Section: Chapter Questions
Problem 32.6QAP
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Question
![On a page titled Correct Separation Scheme print/draw a correct separation scheme to
isolate your molecule from the provided second molecule. Make sure to indicate the phase
of each chemical in every step (s, 1, g, aq) and write the separation technique used in each
step (ie: vacuum filtration). The list below gives the reagents available in the lab. Use any
of the reagents below to isolate the compounds. Remember that the simplest separation
scheme is the best one. Try to avoid unnecessary steps.
10% aqueous NAOH
5% aqueous NaHCO3
H2O
H3PO4
6M HCI
anhydrous Na,SO4
anhydrous MgSO4
Saturated NaCl
5% HCI
Diethyl ether (ether)
CH3OH
lithium aluminum hydride (LiAlIH4)
Sodium borohydride (NaBH4)
NaCl solid](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fc9819384-7ac8-4a35-b95a-106c2e89eec6%2F9007126a-fc1c-4d88-bc8f-f353eb8774a2%2Fgqrjzku_processed.jpeg&w=3840&q=75)
Transcribed Image Text:On a page titled Correct Separation Scheme print/draw a correct separation scheme to
isolate your molecule from the provided second molecule. Make sure to indicate the phase
of each chemical in every step (s, 1, g, aq) and write the separation technique used in each
step (ie: vacuum filtration). The list below gives the reagents available in the lab. Use any
of the reagents below to isolate the compounds. Remember that the simplest separation
scheme is the best one. Try to avoid unnecessary steps.
10% aqueous NAOH
5% aqueous NaHCO3
H2O
H3PO4
6M HCI
anhydrous Na,SO4
anhydrous MgSO4
Saturated NaCl
5% HCI
Diethyl ether (ether)
CH3OH
lithium aluminum hydride (LiAlIH4)
Sodium borohydride (NaBH4)
NaCl solid
![Incorrect Separation Scheme
NH2
ether, 10 % NaOH
ether
aq
NH
6 M HC1
Na,SO4. gravity filtration
vacuum filtration
ether
aq
NaCl
Na SO, 10H,O
NH2
distillation
fraction 1
fraction
ether](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fc9819384-7ac8-4a35-b95a-106c2e89eec6%2F9007126a-fc1c-4d88-bc8f-f353eb8774a2%2Flr1d2en_processed.jpeg&w=3840&q=75)
Transcribed Image Text:Incorrect Separation Scheme
NH2
ether, 10 % NaOH
ether
aq
NH
6 M HC1
Na,SO4. gravity filtration
vacuum filtration
ether
aq
NaCl
Na SO, 10H,O
NH2
distillation
fraction 1
fraction
ether
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