In this experiment products 2, 3 and 4 are produced in slightly different amounts in the three fractions you collect. You are able to quantify the amount of 2 and 3 by examining the 'H-NMRS for each fraction. Before you can do this you should be able to recognise what you expect to observe in the olefinic region of the NMR. OH OH „CH3 „CH3 85% H3PO4, heat CH3 CH2 CH2 Mechanism? trans-1 cis-1 2 3 4 Q1) Fill in the Table 1 with respect to how you expect the olefinic part of the molecules to appear in 2, 3 and 4. · Table 1 molecule Number of olefinic Hydrogens Number of signals Multiplicity 2 3 4

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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In this experiment products 2, 3 and 4 are produced in slightly different amounts in the three fractions
you collect. You are able to quantify the amount of 2 and 3 by examining the 'H-NMRS for each fraction.
Before you can do this you should be able to recognise what you expect to observe in the olefinic region
of the NMR.
OH
OH
.CH3
CH3
85% H3PO4, heat
.CH3
CH2
CH2
Mechanism?
trans-1
cis-1
4
Q1)
Fill in the Table 1 with respect to how you expect the olefinic part of the molecules to
appear in 2, 3 and 4. ·
Table 1
molecule
Number of olefinic Hydrogens
Number of signals
Multiplicity
2
3
4
Transcribed Image Text:In this experiment products 2, 3 and 4 are produced in slightly different amounts in the three fractions you collect. You are able to quantify the amount of 2 and 3 by examining the 'H-NMRS for each fraction. Before you can do this you should be able to recognise what you expect to observe in the olefinic region of the NMR. OH OH .CH3 CH3 85% H3PO4, heat .CH3 CH2 CH2 Mechanism? trans-1 cis-1 4 Q1) Fill in the Table 1 with respect to how you expect the olefinic part of the molecules to appear in 2, 3 and 4. · Table 1 molecule Number of olefinic Hydrogens Number of signals Multiplicity 2 3 4
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