In the analysis of the authenticity of sodium citrate for injection, the following reactions are carried out: A) Flame yellow B) Coloring the flame brick red C) Precipitation with calcium chloride on cooling D) Precipitation with calcium chloride during boiling

In the analysis of the authenticity of sodium citrate for injection, the following reactions are carried out: A) Flame yellow B) Coloring the flame brick red C) Precipitation with calcium chloride on cooling D) Precipitation with calcium chloride during boiling

Introduction to General, Organic and Biochemistry

11th Edition

ISBN:9781285869759

Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres

Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres

Chapter6: Solutions And Colloids

Section: Chapter Questions

Problem 6.112P: 6-112 List the following aqueous solutions in order of increasing boiling point: 0.060 M glucose...

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Supposed you are in a chemistry laboratory gave you a 500 ml Erlenmeyer flask containing 200 ml of heterogenous liquid mixture. This liquid mixture consists of sodium chloride, water, benzoic acid, is made by combining Mixture A and Mixture B. Mixture A (aqueous mixture): sodium chloride is dissolved in distilled water. Mixture B (organic mixture): benzoic acid, phenol and aniline is dissolved in petroleum ether (a nonpolar solvent). Your task is to separate the components of the heterogenous mixture and identify the components. What wet chemical analysis/qualitative test should be performed to detect the compounds?
A researcher reconstituted a vial of 750 mg Cefuroxime Sodium Powder for Injection with 6mL of sterile water for injection. The reconstituted solution was dark amber-colored solution. The package insert states that solution colors range from clear to yellow depending on concentration, diluent, and storage conditions. The researcher was then hesitant to give the patient the solution due to its unusual dark color. Five portions were taken from a batch of cefuroxime sodium. Prior to testing in the instrument, each part was subjected to one of the following conditions: Conditions Specifications Temperature Portion 1: 8°C ± 2°C Portion 2: 30°C ± 2°C Portion 3: 40°C ± 2°C Light Portion 4: Kept in the dark Portion 5: Exposed to direct sunlight 1. Of the several solutions prepared, which absorbance value results should be compared with each other to answer the questions of the pharmacist? Explain your answer.
Supposed you are in a chemistry laboratory and your CHEF102B teacher gave you a 500 ml Erlenmeyer flask containing 200 ml of heterogenous liquid mixture. This liquid mixture consists of sodium chloride, water, benzoic acid, is made by combining Mixture A and Mixture B. Mixture A (aqueous mixture): sodium chloride is dissolved in distilled water. Mixture B (organic mixture): benzoic acid, phenol and aniline is dissolved in petroleum ether (a nonpolar solvent). Your task is to separate the components of the heterogenous mixture and identify the components.
To analyze an aspirin sample, 0.3470 g of crushed tablets are weighed and treated with 50.00 mL 0.1155 M sodium hydroxide, boiling for 10 minutes. Under these conditions the acid acetylsalicylic (MW, 180) reacts according to: CH3COO-C6H4-COOH + 2 OH- → OH-C6H4-COO- + CH3COO- The excess NaOH is then titrated with 11.5 mL of 0.2100 M HCl. What is the purity of said show ?.
Oral rehydration salts are stated to contain the following components: Sodium Chloride 3.5g Potassium Chloride 1.5g Sodium Citrate 2.9g Anhydrous Glucose 20.0g 8.342 g of oral rehydration salts are dissolved in 500 ml of water. 5 ml of the solution is diluted to 100 ml and then 5 ml is taken from the diluted sample and is diluted to 100 ml. The sodium content of the sample is then determined by flame photometry. The sodium salts used to prepare the mixture were: Trisodium citrate hydrate (C6H5Na3O7, 2H2O) MW 294.1 and sodium chloride (NaCl) NW 58.5. Atomic weight of Na = 23. The content of Na in the diluted sample was determined to be 0.3210 mg/100 ml. Determine the % of stated content of Na in the sample.
Oral rehydration salts are stated to contain the following components: Sodium Chloride 3.5g Potassium Chloride 1.5g Sodium Citrate 2.9g Anhydrous Glucose 20.0g 8.342 g of oral rehydration salts are dissolved in 500 ml of water. 5 ml of the solution is diluted to 100 ml and then 5 ml is taken from the diluted sample and is diluted to 100 ml. The sodium content of the sample is then determined by flame photometry. The sodium salts used to prepare the mixture were: Trisodium citrate hydrate (C6H5Na3O7, 2H2O) MW 294.1 and sodium chloride (NaCl) NW 58.5. Atomic weight of Na = 23. The content of Na in the diluted sample was determined to be 0.3210 mg/100 ml. Determine the % of stated content of Na in the sample. The stated should be 104.5, how??
Materials Needed solid I2 solid CUSO4-5H20 food dye solid (NH4)2SO4 heavy metals waste container halogenated waste container non-halogenated waste container semi-micro test tubes and rack regular test tubes and rack squash pipettes acetone cyclohexane propan-2-ol Method Part A: Solubility of ionic and molecular solids 1. Place a small amount (about the size of 1 grain of rice, see picture) of copper sulfate into each of three DRY semi-micro test tubes. Add 20 drops of water to the first test tube and gently flick the test tube with your finger to ensure mixing. 2. Repeat step 1 using acetone in place of water as the solvent in the second test tube. 3. Repeat step 2 replacing acetone with cyclohexane in the third test tube. Hold the test tubes against a white background to compare the solubility of copper sulfate in the three solvents and record your results. Discard these mixtures into the heavy metals waste container in the fume cupboard. Once these test tubes have been emptied you…
A phamacist reconstituted a vial of 750 mg Cefuroxime Sodium Powder for Injection with 6mL of sterile water for injection. The reconstituted solution was dark amber-colored solution. The package insert states that solution colors range from clear to yellow depending on concentration, diluent, and storage conditions. The pharmacist was then hesitant to give the patient the solution due to its unusual dark color. Five portions were taken from a batch of cefuroxime sodium. Prior to testing in the instrument, each part was subjected to one of the following conditions: Conditions Specifications Temperature Portion 1: 8°C ± 2°C Portion 2: 30°C ± 2°C Portion 3: 40°C ± 2°C Light Portion 4: Kept in the dark Portion 5: Exposed to direct sunlight a. Which form of the product – the powder for injection, the reconstituted product, or both – will you subject to the following conditions and why? b. Will you also expose the reference standard of cefuroxime sodium to the same…
6-112 List the following aqueous solutions in order of increasing boiling point: 0.060 M glucose (C6H12O6), 0.025 M LiBr, and 0.025 M Zn(NO3)2.Assume complete dissociation of any salts.
6-78 (Chemical Connections 6A) Oxides of nitrogen (NO, NO2,N2O3) are also responsible for acid rain. Which acids can be formed from these nitrogen oxides?
- Calculate the concerntration of NaOH in the solution provided.
Since CO2 makes up 0.0355% of the atmosphere (on the average) calculate the molar fraction of [CO2•H2O] in the unpolluted rain water (please use constants in table attached)