i) What two criteria should you ensure about your melting point sample before you fill the melting point capillary? j) After filling the capillary, what do you do to avoid air pockets? k) You accidentally overshoot the melting point of Z and the sample melts before you get a reading. Why should you not just wait for it to cool down and redo the determination with the same sample?
i) What two criteria should you ensure about your melting point sample before you fill the melting point capillary? j) After filling the capillary, what do you do to avoid air pockets? k) You accidentally overshoot the melting point of Z and the sample melts before you get a reading. Why should you not just wait for it to cool down and redo the determination with the same sample?
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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