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H₂ `N Br CH3 sion: DMSO 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 f1 (ppm) 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 -0 -5000

H₂ `N Br CH3 sion: DMSO 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 f1 (ppm) 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 -0 -5000

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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H₂ N Br CH3 Discussion: DMSO 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 f1 (ppm) 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 -0 -5000
Transcribed Image Text:H₂ N Br CH3 Discussion: DMSO 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 f1 (ppm) 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 -0 -5000
'H NMR and ¹³C NMR Assignment (20 pts) Assign the 'H NMR and ¹3C NMR signals by filling in the corresponding blanks. Discuss how each spectrum ('H & ¹3C) can be used to help prove the identity of the product. Consider the structural features (chemical shifts and presence or absence of signals) and the number of protons (integration) in the product compared to the starting material. H² H³ 10.0 Discussion: 요 N-H Br CH3 H² H³ 9.0 3.96 8.0 7.0 6.0 5.0 f1 (ppm) H₂O DMSO 4.0 3.0 3.10- 2.0 1.0 -2500 -2000 1500 1000 --500 0.0
Transcribed Image Text:'H NMR and ¹³C NMR Assignment (20 pts) Assign the 'H NMR and ¹3C NMR signals by filling in the corresponding blanks. Discuss how each spectrum ('H & ¹3C) can be used to help prove the identity of the product. Consider the structural features (chemical shifts and presence or absence of signals) and the number of protons (integration) in the product compared to the starting material. H² H³ 10.0 Discussion: 요 N-H Br CH3 H² H³ 9.0 3.96 8.0 7.0 6.0 5.0 f1 (ppm) H₂O DMSO 4.0 3.0 3.10- 2.0 1.0 -2500 -2000 1500 1000 --500 0.0
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given commpound is P-bromoacetanilide

sites of unsaturation in given compound is 5 detail explanation is given in step 2

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