Given a cycloadduct product weight of 2.17 grams, calculate the theoretical yield of this experimental reaction, then use that to calculate %percentage yield of cyclo adduct product.

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Given a cycloadduct product weight of 2.17 grams, calculate the theoretical yield of this experimental reaction, then use that to calculate %percentage yield of cyclo adduct product.

Experiment: Diels-Alder (D-A)
Title: Diels-Alder Reaction (Otto and Kurt). Cycloaddition of Maleic Anhydride with Anthracene
Ref: Hill, R. K.; Barbaro, J. Experiments in Organic Chemistry (2000, 2nd Ed) pp E7-1-3.
Purpose: Synthesize 9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylic anhydride
reflux
Reagent table:
revised 03/09/2010ssh
reagent (source)
Mwt
mp °C bp oC
(Fp).
mmol mass(%)
density
volume
anthracene
178.23 216-8
(121)
10.1
1.84 g (98%)
-
(Acros)
maleic anhydride
(Acros)
98.06
54-56 200
(103)
10.1
1.00 g (99%)
toluene (anhyd.)
(Pharmaco)
111
0.87
43mL
cycloadduct
276.29 261-2
10.1
2.79 g
Transcribed Image Text:Experiment: Diels-Alder (D-A) Title: Diels-Alder Reaction (Otto and Kurt). Cycloaddition of Maleic Anhydride with Anthracene Ref: Hill, R. K.; Barbaro, J. Experiments in Organic Chemistry (2000, 2nd Ed) pp E7-1-3. Purpose: Synthesize 9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylic anhydride reflux Reagent table: revised 03/09/2010ssh reagent (source) Mwt mp °C bp oC (Fp). mmol mass(%) density volume anthracene 178.23 216-8 (121) 10.1 1.84 g (98%) - (Acros) maleic anhydride (Acros) 98.06 54-56 200 (103) 10.1 1.00 g (99%) toluene (anhyd.) (Pharmaco) 111 0.87 43mL cycloadduct 276.29 261-2 10.1 2.79 g
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