Font Paragraph Styles Write Up Sheet for Multi-step Synthesis Experiment 1) Write the reaction scheme (starting material(s), reagents, expected product) for the complete multi-step synthesis of your target molecule. Solvents and catalysts should be included, though "work up" steps need not be shown. Br Br OH 10% (w/v) Br2 HO, TSOH OCH3 HOAC H3CO CH;OH H3CO H3CO Reflux 2) Classify the reaction involved in each step of your multi-step synthesis using one of the following terms: acylation alkylation electrophilic substitution nucleophilic addition oxidation reduction Step 1: Step 2: 3) What isolation technique (suction filtration, extraction, etc.) do you expect to use to isolate the product in each step. See problem 5 below, i e. literature melting point data, to assist with this assessment Step 1: Step 2:
Font Paragraph Styles Write Up Sheet for Multi-step Synthesis Experiment 1) Write the reaction scheme (starting material(s), reagents, expected product) for the complete multi-step synthesis of your target molecule. Solvents and catalysts should be included, though "work up" steps need not be shown. Br Br OH 10% (w/v) Br2 HO, TSOH OCH3 HOAC H3CO CH;OH H3CO H3CO Reflux 2) Classify the reaction involved in each step of your multi-step synthesis using one of the following terms: acylation alkylation electrophilic substitution nucleophilic addition oxidation reduction Step 1: Step 2: 3) What isolation technique (suction filtration, extraction, etc.) do you expect to use to isolate the product in each step. See problem 5 below, i e. literature melting point data, to assist with this assessment Step 1: Step 2:
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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### Write-Up Sheet for Multi-step Synthesis Experiment
**1) Write the reaction scheme (starting material(s), reagents, expected product) for the complete multi-step synthesis of your target molecule. Solvents and catalysts should be included, though “work up” steps need not be shown.**
![Chemical Reaction Scheme]
- Starting Material:
- A benzene ring with a methoxy group (-OCH3) and a hydroxyl group (-OH) attached (starting material on the left).
- Step 1 Reagents:
- 10% (w/v) Bromine (Br2) in acetic acid (HOAC).
- Intermediate Product:
- A benzene ring with a methoxy group and two bromine atoms ortho to the methoxy group, one hydroxyl group para to the methoxy group, and one free carboxyl group (COOH).
- Step 2 Reagents:
- Tosic acid (TsOH) in methanol (CH3OH) with reflux conditions.
- Final Product:
- A benzene ring with a methoxy group ortho to a carboxyl group (COOH) and a bromine atom para to the carboxyl group, and one free hydroxyl group para to the methoxy group.
**2) Classify the reaction involved in each step of your multi-step synthesis using one of the following terms:**
*acylation | alkylation | electrophilic substitution | nucleophilic addition | oxidation | reduction*
- Step 1: ___________________________
- Step 2: ___________________________
**3) What isolation technique (suction filtration, extraction, etc.) do you expect to use to isolate the product in each step. See problem 5 below, i.e., literature melting point data, to assist with this assessment**
- Step 1: ___________________________
- Step 2: ___________________________
---
This document is designed to guide students through a multi-step synthesis experiment. It involves identifying and classifying the chemical reactions in each step and selecting appropriate isolation techniques. It provides a clear and structured approach for educational purposes in a chemistry laboratory course.](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fee4db724-fab1-4de8-a5bb-2f3ff9c611c5%2F6ea27f30-34b8-4de6-a754-e9dd297dffea%2Fqkifskk_processed.jpeg&w=3840&q=75)
Transcribed Image Text:---
### Write-Up Sheet for Multi-step Synthesis Experiment
**1) Write the reaction scheme (starting material(s), reagents, expected product) for the complete multi-step synthesis of your target molecule. Solvents and catalysts should be included, though “work up” steps need not be shown.**
![Chemical Reaction Scheme]
- Starting Material:
- A benzene ring with a methoxy group (-OCH3) and a hydroxyl group (-OH) attached (starting material on the left).
- Step 1 Reagents:
- 10% (w/v) Bromine (Br2) in acetic acid (HOAC).
- Intermediate Product:
- A benzene ring with a methoxy group and two bromine atoms ortho to the methoxy group, one hydroxyl group para to the methoxy group, and one free carboxyl group (COOH).
- Step 2 Reagents:
- Tosic acid (TsOH) in methanol (CH3OH) with reflux conditions.
- Final Product:
- A benzene ring with a methoxy group ortho to a carboxyl group (COOH) and a bromine atom para to the carboxyl group, and one free hydroxyl group para to the methoxy group.
**2) Classify the reaction involved in each step of your multi-step synthesis using one of the following terms:**
*acylation | alkylation | electrophilic substitution | nucleophilic addition | oxidation | reduction*
- Step 1: ___________________________
- Step 2: ___________________________
**3) What isolation technique (suction filtration, extraction, etc.) do you expect to use to isolate the product in each step. See problem 5 below, i.e., literature melting point data, to assist with this assessment**
- Step 1: ___________________________
- Step 2: ___________________________
---
This document is designed to guide students through a multi-step synthesis experiment. It involves identifying and classifying the chemical reactions in each step and selecting appropriate isolation techniques. It provides a clear and structured approach for educational purposes in a chemistry laboratory course.
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