Experiment: Extraction of Eugenol For analysis of medicinal values, the essential constituents are m-Eugenol i.e. 3-Allyl-6- methoxyphenol (69.43%), Eugenol acetate (10.78%), Caryophyllene (6.80%), 2-Pentanone (7.78%) etc. Mass of Cloves: 25.021 grams Mass of Eugenol Recovered: 10.560 grams Mass of Acetyl Eugenol Recovered: 1.416 grams
Experiment: Extraction of Eugenol For analysis of medicinal values, the essential constituents are m-Eugenol i.e. 3-Allyl-6- methoxyphenol (69.43%), Eugenol acetate (10.78%), Caryophyllene (6.80%), 2-Pentanone (7.78%) etc. Mass of Cloves: 25.021 grams Mass of Eugenol Recovered: 10.560 grams Mass of Acetyl Eugenol Recovered: 1.416 grams
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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please help calculate 1-3 using given data

Transcribed Image Text:### Experiment: Extraction of Eugenol
#### Introduction
The extraction of Eugenol is a common experiment conducted to analyze the medicinal values of this essential oil and its constituents. In this specific experiment, the main components to be identified include:
- m-Eugenol (3-Allyl-6-methoxyphenol) which makes up 69.43%
- Eugenol acetate (10.78%)
- Caryophyllene (6.80%)
- 2-Pentanone (7.78%)
- And other minor components
#### Materials
- Cloves: 25.021 grams
- Solvent/extraction medium used (not specified in the document)
#### Process and Results
The key results obtained from this extraction experiment include:
- **Mass of Cloves**: 25.021 grams
- **Mass of Eugenol Recovered**: 10.560 grams
- **Mass of Acetyl Eugenol Recovered**: 1.416 grams
#### Conclusion
This experiment highlights the efficiency of the extraction process for isolating Eugenol and its derivatives from cloves. The data gathered will contribute to further understanding the medicinal properties of these compounds.
---
*Note: There are no accompanying graphs or diagrams referenced or included in the document provided.*
![### Calculations
1. **Calculate the percent recovery of eugenol**:
\[(\text{mass eugenol} / \text{mass cloves}) \times 100 \%\].
2. **Calculate the percent recovery of acetyleugenol**.
3. **Calculate the percent recovery of both acetyleugenol and eugenol**.
### Questions
1. **Describe in words where the eugenol and the acetyleugenol are during each of the extraction steps. Include separation and recovery steps. Put the picture above into your own words.**
2. **What structural difference allows the separation of eugenol from acetyleugenol? Draw the reaction of eugenol with NaOH and show the product obtained.**
3. **Do the online quiz for assigning spectra. Do not scan in spectra!**
4. **What spectral features (from all spectra) allow you to distinguish between eugenol and acetyleugenol?**](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fc02bfde4-a78d-4551-93f6-03d589a5c8dc%2Fdb305d81-bc41-46fb-8e98-8833b7197269%2Ffyait5g_processed.jpeg&w=3840&q=75)
Transcribed Image Text:### Calculations
1. **Calculate the percent recovery of eugenol**:
\[(\text{mass eugenol} / \text{mass cloves}) \times 100 \%\].
2. **Calculate the percent recovery of acetyleugenol**.
3. **Calculate the percent recovery of both acetyleugenol and eugenol**.
### Questions
1. **Describe in words where the eugenol and the acetyleugenol are during each of the extraction steps. Include separation and recovery steps. Put the picture above into your own words.**
2. **What structural difference allows the separation of eugenol from acetyleugenol? Draw the reaction of eugenol with NaOH and show the product obtained.**
3. **Do the online quiz for assigning spectra. Do not scan in spectra!**
4. **What spectral features (from all spectra) allow you to distinguish between eugenol and acetyleugenol?**
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