Draw the mechanism for the friedel crafts reaction of 4 - phenylbutyric acid to alpha tetralone with methanesulfonic MeSO H 3 acid as the catalyst 85-100® C OH MeSO H 85-100 °C
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- Show how the synthetic scheme developed in Problem 23.67 can be modified to synthesize this triiodobenzoic acid X-ray contrast agent.When 4-dimethylaminopyridine (DMAP) is added in catalytic amounts to acetic anhydride and an alcohol, it significantly increases the rate of ester formation. The process begins with a reaction between acetic anhydride and DMAP to form a highly reactive acetylpyridinium intermediate that is more reactive than acetic anhydride itself. Propose a mechanism for this process that includes the formation and reaction of the acetylpyridinium intermediate.4-dimethylaminopyridine (4-DMAP) is a good catalyst for acylation of 2° alcohols
- Nitration of methyl benzoate: Weight of filler paper: 0.682g Mp product: 76-77 C Nitration of Acetanilide: Weight of filler paper: 0.691g Weight of filler paper product: 1.232g Mp product: 212-214 C Compound MM (g/mol) ortho mp (oC) meta mp (oC) para mp (oC) Nitroacetanilide 180.16 94 155 214-217 Methyl nitrobenzoate 181.15 -13 78-80 94-96 Theoretical yield of acetanilde: 0.6664g Theoretical yield of methyl benzoate: 0.7317g find theoretical yield of methyl nitrobenzoate percent yield of your methyl nitrobenzoate and melting point of your methyl nitrobenzoateHow is this compound synthesized with its reaction mechanismNone