Determining Equilibrium concentration for enol and keto from this NMR spectra

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Determining Equilibrium concentration for enol and keto from this NMR spectra

acac in CD3cn at 37.4 oc
H NMR
Current Data Parameters
18mar15jalal
658
1
NAME
EXPNO
PROCNO
F2 - Acquisition Parameters
Date
Time
INSTRUM
PROBHD
PULPROG
20180401
14.37
spect
5 mm PABBO BB/
zg30
19998
TD
SOLVENT
NS
DS
SWH
FIDRES
CD3CN
4
1ccco.000 Hz
C.500050 Hz
C.9999000 sec
13.83
50.000 usec
6.50 usec
310.6 K
1.ccc00000 sec
1
AQ
RG
DW
DE
TE
D1
TDC
==------
SFO1
NUC1
P1
PLW1
CHANNEL fl ========
50C.1344108 MHz
1H
10.60 usec
17.39999962 W
--
F2 - Processing parameters
SI
SF
WDW
32768
500.1290016 MHz
EM
20 19
18
17 16
15 14 13
12 11
10
9
8
7
6
5
4
3
2 ppm
SSB
LB
GB
PC
O Hz
2.00
- 17.6086
m60'L
7.6341
-6.0926
5.6294
5.3222
4.1779
-4.1203
4.0472
3.2423
Transcribed Image Text:acac in CD3cn at 37.4 oc H NMR Current Data Parameters 18mar15jalal 658 1 NAME EXPNO PROCNO F2 - Acquisition Parameters Date Time INSTRUM PROBHD PULPROG 20180401 14.37 spect 5 mm PABBO BB/ zg30 19998 TD SOLVENT NS DS SWH FIDRES CD3CN 4 1ccco.000 Hz C.500050 Hz C.9999000 sec 13.83 50.000 usec 6.50 usec 310.6 K 1.ccc00000 sec 1 AQ RG DW DE TE D1 TDC ==------ SFO1 NUC1 P1 PLW1 CHANNEL fl ======== 50C.1344108 MHz 1H 10.60 usec 17.39999962 W -- F2 - Processing parameters SI SF WDW 32768 500.1290016 MHz EM 20 19 18 17 16 15 14 13 12 11 10 9 8 7 6 5 4 3 2 ppm SSB LB GB PC O Hz 2.00 - 17.6086 m60'L 7.6341 -6.0926 5.6294 5.3222 4.1779 -4.1203 4.0472 3.2423
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