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Determine the structure of the unknown compound by using the spectroscopic data provided. Justify your answer by indicating the relevant supporting information from each spectrum.

Determine the structure of the unknown compound by using the spectroscopic data provided. Justify your answer by indicating the relevant supporting information from each spectrum.

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Determine the structure of the unknown compound by using the spectroscopic data provided. Justify your answer by indicating the relevant supporting information from each spectrum.

1630 IR Spectrum (liquid film) 1680 3000 2000 1600 1200 800 0.0 4000 V v (cm1) (ст 100 Mass Spectrum 0.5 77 131 80 M+ 132 103 60 1.0 40 UV spectrum 20 0.372 mg / 10 mls path length : 0.2cm 1.5 solvent : methanol 40 80 120 160 200 240 280 200 250 300 350 m/e 2 (nm) % of base peak absorbance
Transcribed Image Text:1630 IR Spectrum (liquid film) 1680 3000 2000 1600 1200 800 0.0 4000 V v (cm1) (ст 100 Mass Spectrum 0.5 77 131 80 M+ 132 103 60 1.0 40 UV spectrum 20 0.372 mg / 10 mls path length : 0.2cm 1.5 solvent : methanol 40 80 120 160 200 240 280 200 250 300 350 m/e 2 (nm) % of base peak absorbance
13C NMR Spectrum Resolves into (50.0MHZ, CDCI, solution) two signals at higher field expansion 150 130 ppm сн4 DEPT CH2 CH31 - Resolves into two signals at higher field expansion proton decoupled 150 130 ppm solvent 200 160 120 80 40 8 (ppm) H NMR Spectrum (200 MHz, CDCI, solution) expansion 9.0 8.0 7.0 ppm 1 8 (ppm) 10 8 5 3 2.
Transcribed Image Text:13C NMR Spectrum Resolves into (50.0MHZ, CDCI, solution) two signals at higher field expansion 150 130 ppm сн4 DEPT CH2 CH31 - Resolves into two signals at higher field expansion proton decoupled 150 130 ppm solvent 200 160 120 80 40 8 (ppm) H NMR Spectrum (200 MHz, CDCI, solution) expansion 9.0 8.0 7.0 ppm 1 8 (ppm) 10 8 5 3 2.
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